A fast run Down of my S to B extraction please help

[fun_guy88]

Hello every one I just want to run this down and help me answer any questions i have so here we go!

I am doing a S to B extraction so I took a LB of MHRB and crushed it up...not powder fine but still pretty good. put that in a large wine glass jug with water and one LB of LYE

then shake and letting it sit in a hot water bath for a few hours and adding VM&P the that solution shake jug and suck out the VM&P and add to a collection jug

then from there make a mixture of PH plus and water and ad that to the collection jug quickly shake and separate the two layers and do that about 3 or 4 times until most of the impurities are gone.

following that take some epson salt and cook it in the microwave for a little while take a chunk of that drop it into the new collection jug shake a little bit and then quickly separate the two layers that form.

No once the solution has been washed and dryed have it in the freezer for about 72 hours and allow to freeze into crystials

This is where I get lost....

What are the best ways to get the product out of solvent.....then also how do i go about doing a recrystallization do I then take my crystals heat up more VM&P drop the crystals in than and allow it to freeze again?

Any tips or anything would be a huge help thank you so much!

 

[Ice House]

OMG I need help

So I had my mason jars with 400 ml of liquid each in them left in the freezer for about 3 or 4 days after that I opened them up and dumped it out into a baking dish and put a fan in front of it.... Now all im left with is yellow goo that looks and smells like spice but its not turning crystals or powder its just staying goo like. its been in front of the fan for about 8 hours now do you think it just needs more time?

I would take some solvent, either Naphtha or Heptane, warm it up in a warm water bath and put enough of it into the baking dish to dissolve everything. Dont put TOO MUCH in. Put just enough in to completely dissolve everything.

now.. at this point you have 2 options. 1. put it back into a baking dish and slowly evap and you should get some xtals forming. 2. you can put it into a small jar or glass container with a lid and let it cool to room temp first, cool it in the fridge second and then put it into the freezer and let it sit for a day or two.

Sounds like you need to use the Wiki and follow the correct procedures for this type of extraction. FOLLOW THE RECCOMENDED STEPS TO THE LETTER!!!!!! Do not DEVIATE!!!!

You used way too much solvent in your jars and thats allot of solvent to try and evap in short order. USE LESS solvent next time and do more pulls. The reason there was nothing in them when you took them out of the freezer is because you had TOO much solvent in them.

The only way it would have precipitated out in the freezer is if you would have evaped some of the solvent off first making the DMT to solvent ratio higher.

Make sense?

Read the FAQ and Wiki sections for more help.

STB is as simple as it gets.

good luck