Before i do this, i want to make sure im doing it right. STB

[Darion321]

OK so in laymans terms this is what im doing.

Adding 100g of lye to 1500 ml of distilled water. Shake vigorously for 1 min.
Add 100g of powdered bark and shake for 5 more min.
Let the jar sit for an hour or 2 to let the naptha go to the top.
Use a sep funnel to put naptha in new jar.
With the same mush of MHRB add more naptha to it and take out the naptha into 3 more jars.
Put the naptha in the freezer over night.
Use a pipette to take the naptha out of jars and let the rest of the naptha evaporate off the jars.
Once the jars are ready scrape the DMT crystals off the jar into a storage container.
Dissolve the crystals into HEPTANE and freeze precipitate again.
Scrape the crystals and go straight to smoking or recrystallize them.

Please tell me if this is right and need to make any changes.

 

[actualfactual]

you won't be able to use a sep. funnel for this (naphtha is on top of the thick basey soup). you decant the naphtha from the top using a pipette or baster

 

[Darion321]

Yea i kind of realized about 10 min ago. But as for everything else its right?

 

[The Day Tripper]

I wouldn't shake a jar/container of naoh dissolving in water. The reaction releases heat/vapor, and i think its much safer to just stir it while having it sit in a sink. Naoh dissolves pretty fast in water, and simple stirring will suffice, with out the risk of catastrophic accidents that could end very very bad using sealed containers and shaking.

Just a heads up. Everything else looks good though, good luck.