KUSHMASTER
Rising Star
Hello Nexus! I was planning on setting up a bufo extract but wanted to find out from my mentors if this tek I put together (by collecting info here on the nexus..) would suffice. Any help or constructive criticism?
(EDIT= I've changed a couple things that were recommended.)
Accquire:
50gms A. Colubrina Seeds
Xylene
Acetone
Citric Acid
Sodium Carbonate
1. Grind 50gms seeds and toast at 300F for 60min.
Then repeatedly wash with 250ml cold xylene until it pulls clear
repeat this^^ with 200ml acetone until that pulls clear. discard solvents.
2. Freebase seed powder with Sodium Carbonate (half the weight of the seeds) and little water to form a paste, mix for 10 min then make sure mix is completely dry. Bake in oven at 300F for 60min.
3. Collect mix and Start doing pulls with 200ml acetone and then separate solid, combining your pulls together.
4. Add 10% Citric Acid Saturated Acetone ( 10gms Citric Acid to 100ml of acetone) to combined acetone pulls to drop bufo citrate and other crap. Keep adding CASA until nothing else precipitations complete.
Those four steps are JUST for getting rid of fats and oils.
5. Freebase bufocrap citrate with sodium carbonate (equal to the weight of the Bufocrap) and little water to form a paste, mix for 10 min and let it dry completely. Bake in 300F oven for 60min.
6. Collect from oven and begin pulls with acetone. Combine Acetone pulls and evaporate
(this will separate the any excess sodium carbonate and other solid left overs)
7. Boil the bufo-goo thats left over from acetone pulls with 100ml of xylene for 5 minutes. Carefully/Quickly pour boiling xylene into new jar before it starts to cool. Be sure to leave the goo-gunk in the bottom.
Those three steps are to separate the bufo alkaloid from the other nauseating substances and most other random solids that are present
8. Once xylene sits for enough time to completely cool, your extract drops out. With care, decant Xylene and scrape crystals off inside of jar.
9. Dissolve Extract in acetone to break it down, let it evaporate and scrap em up
10. Once dry, Bake end product 1 more time at 300F for 60min.<(probly not necessary) Scrape up your baked extract and subject it to acetone pulls. Collect em and Evap. (Repeat step 7-9 if end product still contains unpleasant/unwanted alkaloids)
Again any help or advice from the more experienced persons would be greatly appreciated! Thanks
(EDIT= I've changed a couple things that were recommended.)
Accquire:
50gms A. Colubrina Seeds
Xylene
Acetone
Citric Acid
Sodium Carbonate
1. Grind 50gms seeds and toast at 300F for 60min.
Then repeatedly wash with 250ml cold xylene until it pulls clear
repeat this^^ with 200ml acetone until that pulls clear. discard solvents.
2. Freebase seed powder with Sodium Carbonate (half the weight of the seeds) and little water to form a paste, mix for 10 min then make sure mix is completely dry. Bake in oven at 300F for 60min.
3. Collect mix and Start doing pulls with 200ml acetone and then separate solid, combining your pulls together.
4. Add 10% Citric Acid Saturated Acetone ( 10gms Citric Acid to 100ml of acetone) to combined acetone pulls to drop bufo citrate and other crap. Keep adding CASA until nothing else precipitations complete.
Those four steps are JUST for getting rid of fats and oils.
5. Freebase bufocrap citrate with sodium carbonate (equal to the weight of the Bufocrap) and little water to form a paste, mix for 10 min and let it dry completely. Bake in 300F oven for 60min.
6. Collect from oven and begin pulls with acetone. Combine Acetone pulls and evaporate
(this will separate the any excess sodium carbonate and other solid left overs)
7. Boil the bufo-goo thats left over from acetone pulls with 100ml of xylene for 5 minutes. Carefully/Quickly pour boiling xylene into new jar before it starts to cool. Be sure to leave the goo-gunk in the bottom.
Those three steps are to separate the bufo alkaloid from the other nauseating substances and most other random solids that are present
8. Once xylene sits for enough time to completely cool, your extract drops out. With care, decant Xylene and scrape crystals off inside of jar.
9. Dissolve Extract in acetone to break it down, let it evaporate and scrap em up
10. Once dry, Bake end product 1 more time at 300F for 60min.<(probly not necessary) Scrape up your baked extract and subject it to acetone pulls. Collect em and Evap. (Repeat step 7-9 if end product still contains unpleasant/unwanted alkaloids)
Again any help or advice from the more experienced persons would be greatly appreciated! Thanks