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Clean DMT Fumarate powder?

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Hi, I just tried the BLAB tek on Acacia Confusa and got the DMT fumarate like above image.
Initially the product is yellow wax and it's light yellow powder with light smell after I dried it.

I would like to consume it with MAOI at this stage, as I replaced d-limonene with Xylene in the BLAB tek, should I wash it with Acetone or following the instructions to clean it? Is it correct to make the powder color lighter for better(safer?) oral use?

Thanks for any help.
 
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I did that with just anhydrous acetone, getting off-white powder resembling crumbles, still somewhat sour (fumaric acid present).

Instead of doing more washes, I would also re-a/b the product next time. This is best if you aim for purity.

Maybe your product is already good enough - depends on fumaric acid contamination (maybe a pH test will reveal?)

Also depends on solvent purity - have you done evap. test on your xylene?
 
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Bthechange said:
Would you be so kind to provide us with the instructions on your method?
Click to expand...
boil 99% isopropanol ( with plenty ventilation, either outdoors or with giant fans blowing the vapor outdoors) by immersing pyrex glass container (dont use mason jar they crack with heat) in simmering water, hot enough that its near boiling, so that the isopropanol begins to boil.. then add your DMT fumarate, stir while it boils, and add more 99% isopropanol until all the dmt fumarate dissolves

stir for at least 5 min intervals after adding more isopropanol to see how much more dissolves before adding more, since it takes a lot of time to dissolve even when you have enough solvent.

when all dissolved ,should look completely clear, colored yellow with impurity

put somethign overtop to slow evaporation and allow it to cool down to room temperature while disturbing as little as possible. What can happen can vary here sometimes depending on how concentrated it is.. the first crop of dmt fumarate can crystallized out and bring a lot of the yellow color back out, you are left with a colorless solution, put that solution in the freezer for 3-4 days, and it will give you a second smaller crop of highly pure colorless dmt fumarate, you can repeat the process with the yellow fumarate if you like even decolorize with activated carbon if you are ok with losing some yield
 
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Mindlusion said:
boil 99% isopropanol ( with plenty ventilation, either outdoors or with giant fans blowing the vapor outdoors) by immersing pyrex glass container (dont use mason jar they crack with heat) in simmering water, hot enough that its near boiling, so that the isopropanol begins to boil.. then add your DMT fumarate, stir while it boils, and add more 99% isopropanol until all the dmt fumarate dissolves

stir for at least 5 min intervals after adding more isopropanol to see how much more dissolves before adding more, since it takes a lot of time to dissolve even when you have enough solvent.

when all dissolved ,should look completely clear, colored yellow with impurity

put somethign overtop to slow evaporation and allow it to cool down to room temperature while disturbing as little as possible. What can happen can vary here sometimes depending on how concentrated it is.. the first crop of dmt fumarate can crystallized out and bring a lot of the yellow color back out, you are left with a colorless solution, put that solution in the freezer for 3-4 days, and it will give you a second smaller crop of highly pure colorless dmt fumarate, you can repeat the process with the yellow fumarate if you like even decolorize with activated carbon if you are ok with losing some yield
Click to expand...
Thank you 🙏 🕉️
 
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