Questfinder
Rising Star
Well it's been a rollercoaster of a day, this extraction has been a trip in itself. I started about 8 hours ago having had not enough sleep for many days, and not enough to eat either really, which only added to the ride.
I started out following Vovin's tek (after reading just about all of them, I liked this one the best), but because of how tired I was and unsure of everything I became (it all seemed too good to be true, still does quite frankly) I ended up skipping the first defatting step and only basified the first acid wash, and only did one solvent pull on that, which also as it turned out I used way too much solvent (50g:60mL). When I separated it into the baking dish there was none of this cloudy business going on that I'd heard of so often, and so longed to see.... Alas I thought I was doomed. Bad bark, I'd done something wrong, bad luck yet again. But, here I am half hour later, armed with the information I had used to much solvent. I set off back down the stairs again trying to keep hope in check so as not to be disappointed. I blew on the solvent gently, nothing. Again, for a little longer, ooh I see something. One last time, ohhh yeah, here we go, a nice thick cloud of DMT swirling about in the naphtha. So the bark is good after all, my process.. Well, worked is the best I can say lol. I have learnt a hell of a lot today, chiefly being that I need some proper glassware if I am to continue my adventure into chemistry. There's a lot of other stuff too, but I'm too tired to continue this post. I just wanted to vent my excitement at the fruits of my labour lol :')
Thanks for everyone's help.
I started out following Vovin's tek (after reading just about all of them, I liked this one the best), but because of how tired I was and unsure of everything I became (it all seemed too good to be true, still does quite frankly) I ended up skipping the first defatting step and only basified the first acid wash, and only did one solvent pull on that, which also as it turned out I used way too much solvent (50g:60mL). When I separated it into the baking dish there was none of this cloudy business going on that I'd heard of so often, and so longed to see.... Alas I thought I was doomed. Bad bark, I'd done something wrong, bad luck yet again. But, here I am half hour later, armed with the information I had used to much solvent. I set off back down the stairs again trying to keep hope in check so as not to be disappointed. I blew on the solvent gently, nothing. Again, for a little longer, ooh I see something. One last time, ohhh yeah, here we go, a nice thick cloud of DMT swirling about in the naphtha. So the bark is good after all, my process.. Well, worked is the best I can say lol. I have learnt a hell of a lot today, chiefly being that I need some proper glassware if I am to continue my adventure into chemistry. There's a lot of other stuff too, but I'm too tired to continue this post. I just wanted to vent my excitement at the fruits of my labour lol :')
Thanks for everyone's help.