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harmala red formation in harmaline crystallization of different alcohols

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AIRDOG

Padawan
Hi... i recently started my exploration in the harmala's realm and changa....

i just need to say WOW, its such an extreme difference between changa and normal DMT, i think im never going back to crystal as the leaf with harmala`s is so much more rewarding.

after trying several extraction methods on red vine... first extraction was standard 3x water boils with the pita filtering and several A/B cycles with vinegar and lye.... using carbonate in the last basification, filtered and evaped to dryness and followed by an acetone pull.... (noticed acetone is the worst of all solvents) with IPA a close second, with ethanol being the best of these 3....

all these solvents produced red freebase as a fine powder... i presume harmala red formation


second extraction was the alcohol/vinegar microwave boil, which i liked the best to be honest, yield is greater filtering easier and end product was cleaner...

after doing 3x pulls inside the microwave with 1:1 vinegar/ethanol mix, reduced the liquid a bit so most of the alcohol was gone and basified with lye.

redissolved resulting red gunk in vinegar and divide the liquid in 2, half of it i tried to perform a manske but utterly failed and the other half i basified with carbonate and pulled with methanol after dryness of base gunk

the methanol final product
 

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