Help attaining lsa in crystalline format (fumarate?)

[panillusionary]

I recently performed a basic lsa extraction using 8 ether washes, and a few IPO washes after. My result was the brown oily, slightly salty (disgusting) ipo seed extract. Very potent, a piece the size of one HBWR seed was sufficient to have me feeling weird as fuck all day, climbing trees, slithering across the floor, and impulsively dancing. Is definitely a strong body high- it also definitely reminded me of and gave flashbacks of being a little kid again who couldn't stay still, can't focus, just wants to play and nap. Was cool, haha.

But I wasn't even thinking I was making this brown gunk. I thought after the IPO had all evaporated I would be left with some clean lsa white crystals.

How can I make lsa crystals out of another batch of HBWR seeds, or further refine my current batch of brown yucky shit.

Anyone who can explain this simply step by step, or give me a link to someone else who already has?

It seems like this brown shit is what everyone has been making, if they aren't putting it into puregrain ethanol ( I don't have any available to me) - Surely there are some smart people here who know how to get around this unatractive gunk and make some real pure lsa from HBWR or MG seeds.

 

[Kash]

You have to remove the impurities before it will crystallize. You can use my tek as a model and adjust it to make a fumarate salt at the end. I theorize after impurities are removed, one could dissolve the freebase in acetone, and then mix with fumaric acetone to precip LSA fumarate, although I am not sure the solubility properties of LSA fumarate in acetone. More work to do on this in the future.

 

[panillusionary]

Hey Kash! Your tek is great and informative, probably the best on the web for making this brown gunk, haha

Thank you for your commitment and interest in lysergic amide. I was reading this thread today in which you had made some comments, benzyme posted a picture of the good lsa crystals I'm interested in.

Pure LSA Extraction - Welcome discussion - Welcome to the DMT-Nexus

That thread is definitely useful, but could you elaborate on how exactly one would remove the impurities?

Acetone does seem like a better candidate than IPO as it is more volatile, and will evaporate faster. I've never actually worked with fumaric acid as i'm not sure where to get or make it.

Thankyou