sweatloaf13
Rising Star
100grams MHRB powdered 2 Vitamin C tablets,1000mg. crushed as fine as possible 1qt of dH20 1 1/2 TBSP. of 100%Roebic Drain Cleaner NaOH(Lye) VM&P Naptha(accept no substitutions!!) Coffee filters,cheesecloth,wire tea strainers Funnel Quart size Mason jar(with lid) Crockpot a couple 1/2 pint mason jars(like you use for growing shrooms) shotglass Pyrex baking dish A freezer/refridgerator a stove pH papers or pen(I don't use,but am picking one up ASAP) Step 1 In your crockpot add 100grams of finely powdered MHRB(adjust amounts accordingly-take size of vessel you will be using into account as well),while also adding 1 finely crushed Vitamin C tablet 1000mg. to 1 quart of warm dH2o.Stir until it is mixed thouroughly.Add 1/2 of this(give or take some)into the crockpot until the MHRB is submerged completely.Do not discard the remaining water/vitamin C solution since it will be used on 2nd extraction.Mix contents up well so the acidic water soaks every bit of bark in there.Set temperature to medium setting for 30-40minutes,stirring regularly.After this time,reduce heat to low or warm setting,and allow to simmer for another 45minutes to an hour.Stir as before. When time has elapsed,strain liquid through a wire strainer into a plastic container.Repeat this a few times using a tea strainer and cheesecloth as well(if available).The basic goal is to remove as much of the plant matter from the liquid as you possibly can.DO NOT toss whatever mucky red slop you collect from the liquid.This is to be collected and tossed back into the crockpot once ALL the liquid has been filtered.Put strained liquid aside.Add remaining 1/2qt. of acidic water to the collected and strained plant matter in the crockpot and simmer on low for 45minutes to an hour,stirring as before.Strain as before and collect.If you want to take the time and squeeze every bit of alkaloid out of your sludge you can do this step one more time using a 1/4qt. solution with 250mg. of vitamin C with the sludge in pot on HIGH for an hour.Strain again and combine 2-3 extractions in one plastic container,making sure it's been strained as thouroughly as possible.Cover container and throw in freezer for 90minutes to cold filter.When removed,there will be a layer of GREY sludge sitting at the bottom.Pour the viscious red liquid into a qt. mason jar and throw the grey shit AWAY. Step 2. In a 1/2pint canning mason jar add 100mL of dH20 and heat in microwave for 90 seconds or so(get it nice and hot).Now,SLOWLY and CAREFULLY stir in(just a little at a time so it doesn't boil over)1 1/2TBSP of NaOH(Lye)to the hot water.Be careful,as a Lye burn is not pleasant.Wear safety goggles and appropriate gloves and avoid any stuipid accidents.It only shines more light on the more careful ones who don't want ANY unnecessary attention or scrupulation.Once your basic solution is ready,slowly pour it into the mason jar with your extractions.The liquid will change from a dark-red,to a grey,and then black.This is what you want.If it's not black the pH is NOT high enough and you will fail.If you have a pH pen or papers you want a 14pH.If you don't have these,you can be sure the measurement I gave(if using 100grams MHRB)will be MORE than sufficient.It's difficult to overdo it,but easier to underdo it.Shoot for the sky!! Cap the lid to jar and upturn the jar(DO NOT SHAKE!!)for a good 3-5min.,loosening the lid when in the upright position periodically to avoid any build-up of pressure!!This is very important.Make sure your goggles and gloves are still on!!! Step 3. In a shotglass pour out about 30-50mL of VM&P Naptha(don't use that zippo/coleman shit-yuck!!)and put to side.In a seperate 1/2pint mason jar,fill it up halfway with tap water(save the distilled)and stick it in your microwave for 2 1/2-3minutes(or until boiling).Carefully remove from microwave,and place the shotglass of Naptha into the jar carefully to avoid cracking glass,making sure water doesn't overflow from sides.Let shotglass sit in this hotwater bath for about 10minutes,or until Naptha is GOOD and HOT.Open Qt.jar and pour in the hot Naptha. Tighten lid and upend as before,for a good 5-10 minutes,ensuring all free-base DMT meets the hot solvent.When finished,place jar down(or for better,faster results)into a hot water bath until layers fully seperate,and no emulsion forms.The crystal clear layer is the solvent,and where all your magic lies.Once fully seperated,this clear layer needs to be carefully removed,and this step repeated an additional 2 more times. Step 4. Using an eyedropper(ideal),empty spore syringe,glass pipette or turkey baster,siphon off as much of the clear solvent layer as you possibly can,making sure NOT to get any of the other layers into the solvent as well.This takes patience and careful work.If using a larger utensil,an eyedropper is best when there isn't much remaining.Deposit siphoned solvent into a clean mason jar.Do this for all 3 pulls.Once the solvent has been collected,cover jar tightly and stick in freezer for 24-48hours.You will see crystals begin to fall out of solvent within a few hours but wait it out.After time has elapsed,over a clean pyrex dish,pour out solvent and whatever crystals follow through a coffee filter.The shards will stick to filter.There should be a substantial amount still sitting at the bottom of your jar.Collect crystals,and allow to air dry.Cover with a paper towel so no dust collects.Pour solvent into a new jar and return to freezer for a few days or evaporate it by air to see what you get. You can recrystallize if desired,though I've found it unecessary. If anyone has anything to add please do!! Props to Condo and Marsofold for showing the way goodluck and be carefull!!! 
