Hello,
I have been using a lye/xylene/HCl extraction for years and had OK luck with it. However I have been toying with the CIELO tek these last few weeks and have a couple of questions I've not found when reading other posts:
1) is anyone else having issue with the citrate crystals become sticky after drying and storing? I am having significant clumping and sticking to the bottom of my storage container. Perhaps it is the unconditioned environment (garage) where they were temporarily stored. Perhaps they are hygroscopic?
2) Separate issue from the above, I have a container with tan HCl crystals which I would like to convert to citrate, but I'd read that lye is too strong a base for use with ethyl acetate. Is it OK to basify these HCl crystals with lime and proceed via CIELO? Or might the lime react strangely with the HCl crystals?
I have been using a lye/xylene/HCl extraction for years and had OK luck with it. However I have been toying with the CIELO tek these last few weeks and have a couple of questions I've not found when reading other posts:
1) is anyone else having issue with the citrate crystals become sticky after drying and storing? I am having significant clumping and sticking to the bottom of my storage container. Perhaps it is the unconditioned environment (garage) where they were temporarily stored. Perhaps they are hygroscopic?
2) Separate issue from the above, I have a container with tan HCl crystals which I would like to convert to citrate, but I'd read that lye is too strong a base for use with ethyl acetate. Is it OK to basify these HCl crystals with lime and proceed via CIELO? Or might the lime react strangely with the HCl crystals?