mescaline sulfate - questions

[Transform]

anyone have information on mescaline tartrate in ethanol 96? I’m gonna experiment a bit with sulfuric acid 30% and tartaric acid with ethanol 96 but would love some information if anyone has it

There's no entry for M tartrate in the CAS listing in the Shulgin Index, so you might be out on a limb there and have to generate your own solubility data. Have you tried looking on PubChem?

Of the Nexians, @Loveall would be the prime candidate for knowing this one.

 

[modern]

Finally got around to making m sulfate. Iso99 cleans and removed excess sulfuric acid. Very pretty needles but this was already quite pure starting material.

Didn’t notice the hot/cold water trait for recrystalizing but was probably due to still having excess sulfuric acid at the time.

 

[modern]

so I finally observed the hot/cold water recrystallization property. It came out to around 100mg/ml hot water solubility and made nice large shards... After a few crystallizations Ill post a photo here.

 

[modern]

Was able to remove a light tan color after a few cold fridge rest saving the water to see if any more can be recovered. Didn’t weight it yet.
If fast crystallization due to being over saturated or moving the liquid it forms thin needles but slow crystallization makes nice flat shards