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mixing batches ...

stolenface

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can saturated heptane be mixed from two seperate batches for a freexe precipitation? so that all your pulls can be precipitated at once?
 
Sure, why not? Though you may benefit from evaporating down a volume of the combined solvent, as it's probably not supersaturated. Will make life easier when freeze precipitating, cause some of the goods will likely not drop out at a certain equilibrium.

Try combining all your questions in one thread next time too, so we can boil em down and answer em in one go ;)
 
ballzdeep1 said:
can saturated heptane be mixed from two seperate batches for a freexe precipitation? so that all your pulls can be precipitated at once?


Sure you can....but my questions is why you are using heptane for pulls? Save that expensive stuff for recrystalizations!
 
no access to naptha- southern CA!!! i actually did notice that the store does carry xylene which i havent been able to find as well ....
 
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