So, I have had good results in the past extracting with a STB method, however, I have let the xtals sit in improper conditions so they have oxidised.
Thusly I am planning to do my first Zinc wash with acetic acid and zinc, then basify and extract with naptha as I would do normally to a STB soup. Right?
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So, my real question is thinking of a new way to include this zinc wash. I have looked into AB teks but am a little confused and put off by the thought of having to boil this solution. I am wondering if someone with experience and/or knowledge could review my idea.
So far my idea is to soak powdered bark in distilled vinegar for 3 days (as suggested on other teks to avoid boiling) then add zinc and stir for a few hours. Then basify with lye or sodium carbonate (which is better?) to a ph of 10 and extract with naptha as a normal stb tek, freeze precipitate e.t.c.
One soup, no filtering, just mix all at right times and non-polar extraction.
This should work right?
Thusly I am planning to do my first Zinc wash with acetic acid and zinc, then basify and extract with naptha as I would do normally to a STB soup. Right?
DMT n-Oxide to freebase. Another pictorial by Nature Boy - The Psychedelic Experience - Shroomery Message Board
Rushing this due to expected power outage any minute now from Hurricane Irene, so forgive me. Will be back to clean it up when I can. Overview: This procedure is essentially an acid-base

So, my real question is thinking of a new way to include this zinc wash. I have looked into AB teks but am a little confused and put off by the thought of having to boil this solution. I am wondering if someone with experience and/or knowledge could review my idea.
So far my idea is to soak powdered bark in distilled vinegar for 3 days (as suggested on other teks to avoid boiling) then add zinc and stir for a few hours. Then basify with lye or sodium carbonate (which is better?) to a ph of 10 and extract with naptha as a normal stb tek, freeze precipitate e.t.c.
One soup, no filtering, just mix all at right times and non-polar extraction.
This should work right?