EDIT: THIS IS THE ORIGINAL EXTRACTION LOG, not the final tek.
The final tek can be found here
SWIM felt it would be nice for SWIY to read his short backstory to appreciate how excited SWIM is about this new-but-many-aspects-borrowed-TEK!
Special thanks to:
amor_fati for his work with lime which changed this tek from good to GREAT!
69ron for his san pedro tek which taught SWIM the power of lime!
Everyone who ever replied to SWIM's posts!!!!
Sap story start:
SWIM has spent the last few months trying to get a good yield of pure white spice.
He started out with A/B w/ lye + naptha and got .1-.2% at was long and a lot of work and not too worth it. (at least at that yield)
He swapped to STB w/ lye + naptha and got .2-.3% SWIM was happy that he could get a better yield with less steps, but he was wondering how people get up to and >1%
SWIM then purchased some xylene because that meant he could change his tek to remove not only heating the lye bark goo.
(Shaking a 60 C gallon glass jar is not that fun, haha)
Although SWIM did try evaporating the xylene it didn't work to quickly. Still gooey after 4 days in summer!
SWIM then spent way too much time making a STB - A/B combo including salting out the freebase then re-freebasing.
The tek was decent. It was a lot of work and yielded .4-.6% But it was pretty dirty most of the time. If the spice was the color of egg-yolks it was a good pull.
Then SWIM started extracting san-pedro and got very interested in LIME.
He read about some TEKs involving lime with MHRB and found they all seemed like much more work than a typical Lye STB and many were made to produce gooey acetates or involved extra steps to non-smokable fumurates.
SWIM felt that he could use this powerful substance to extract freebase DMT and in the end he was suprised just how easy it was!
SWIM started with STB lime and though the yields were decent (.7%) the lime had to sit for over 2 days before a full yield was produced.
Then SWIM came upon "amor_fati's Nontoxic Approach to the Extraction of DMT" and stole the first step and OH MY HAMBERGERS!!! It worked and here is the first test log:
For those of you who don't like stories start here
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"XTRACTION LOG:
Took 30g mhrb and added 50ml heated vinegar.
Put in hot water bath and stirred for ~30-40 min.
Added 50g lime and 36ml water to correct consistancy.
After ~20min pulled off ~20-25ml naptha which after 2 hours in the freezer yielded 75mg pure white spice!!!
After 1 hour (still in hot water bath) added another 25-35 ml naptha. Yielded 45mg
Bear in mind there was probably 5-10mg on left over in each after scraping.
After 1 more hour added ~30-40ml naptha. 65mg
1-2 hours later 60ish ml naptha added and stirred very thouroughly while in bath.
first container = 62mg, second 15mg
SWIM pulled some more naptha in the same manner this morning (+13 hours) and it looks to have 5-10mg left. IE: The other pulls got 98% of it!"
if you add that up plus SWIM give a low estimate of 5mg of freebase residue on the extraction containers. that is 272mg pulled within 4 hours and precipitates for 8 hours.
.277g / 30g = .923% SWIM's highest yield yet, In only 4 hours!
All crystal white!
Here is the 4th pull:
All of the pulls looked like that.
And the jars with residue.
SWIM is about to start a 200g extraction as soon as he goes to the dollar store to get some bowls.
Also, SWIM will try a limonene pull to get the jungle off afte the N-N is gone
Will update!
The final tek can be found here
SWIM felt it would be nice for SWIY to read his short backstory to appreciate how excited SWIM is about this new-but-many-aspects-borrowed-TEK!
Special thanks to:
amor_fati for his work with lime which changed this tek from good to GREAT!
69ron for his san pedro tek which taught SWIM the power of lime!
Everyone who ever replied to SWIM's posts!!!!
Sap story start:
SWIM has spent the last few months trying to get a good yield of pure white spice.
He started out with A/B w/ lye + naptha and got .1-.2% at was long and a lot of work and not too worth it. (at least at that yield)
He swapped to STB w/ lye + naptha and got .2-.3% SWIM was happy that he could get a better yield with less steps, but he was wondering how people get up to and >1%
SWIM then purchased some xylene because that meant he could change his tek to remove not only heating the lye bark goo.
(Shaking a 60 C gallon glass jar is not that fun, haha)
Although SWIM did try evaporating the xylene it didn't work to quickly. Still gooey after 4 days in summer!
SWIM then spent way too much time making a STB - A/B combo including salting out the freebase then re-freebasing.
The tek was decent. It was a lot of work and yielded .4-.6% But it was pretty dirty most of the time. If the spice was the color of egg-yolks it was a good pull.
Then SWIM started extracting san-pedro and got very interested in LIME.
He read about some TEKs involving lime with MHRB and found they all seemed like much more work than a typical Lye STB and many were made to produce gooey acetates or involved extra steps to non-smokable fumurates.
SWIM felt that he could use this powerful substance to extract freebase DMT and in the end he was suprised just how easy it was!
SWIM started with STB lime and though the yields were decent (.7%) the lime had to sit for over 2 days before a full yield was produced.
Then SWIM came upon "amor_fati's Nontoxic Approach to the Extraction of DMT" and stole the first step and OH MY HAMBERGERS!!! It worked and here is the first test log:
For those of you who don't like stories start here
|
|
\/
"XTRACTION LOG:
Took 30g mhrb and added 50ml heated vinegar.
Put in hot water bath and stirred for ~30-40 min.
Added 50g lime and 36ml water to correct consistancy.
After ~20min pulled off ~20-25ml naptha which after 2 hours in the freezer yielded 75mg pure white spice!!!
After 1 hour (still in hot water bath) added another 25-35 ml naptha. Yielded 45mg
Bear in mind there was probably 5-10mg on left over in each after scraping.
After 1 more hour added ~30-40ml naptha. 65mg
1-2 hours later 60ish ml naptha added and stirred very thouroughly while in bath.
first container = 62mg, second 15mg
SWIM pulled some more naptha in the same manner this morning (+13 hours) and it looks to have 5-10mg left. IE: The other pulls got 98% of it!"
if you add that up plus SWIM give a low estimate of 5mg of freebase residue on the extraction containers. that is 272mg pulled within 4 hours and precipitates for 8 hours.
.277g / 30g = .923% SWIM's highest yield yet, In only 4 hours!
All crystal white!
Here is the 4th pull:
All of the pulls looked like that.
And the jars with residue.
SWIM is about to start a 200g extraction as soon as he goes to the dollar store to get some bowls.
Also, SWIM will try a limonene pull to get the jungle off afte the N-N is gone
Will update!
