rescue me? FASW + vinegar+lim pull

[limoseen]

Ok so made a fark up... had a couple of things on the go... did q21q21 tek to the point of salting with vinegar pulls...

So I put these aside and was making some other attempts... I have accidentally put a FASW into the acetate solution intead of the solvent... so of course when I noticed the solution didnt separate I was like uho..

What can I do ??

 

[limoseen]

Ok so I am thinking if I evap it down I will get jimjam fumurate goo/crystals.... I cannot see anyway to leech the spice from one to the other.. any ideas ?

 

[ragabr]

You could rebase, pull with solvent and salt again.

 

[q21q21]

BLAB

step 6 - acetates conversions seems like it would be your best bet.
SWIM has never done it, but it looks quite simple.

 

[limoseen]

I evaped in dehydrator... and its gone to nice jimjam goo... with very very slight crystals... Im thinking that this would be fine for oral use ???

What would the implications for smoking goo with fumarate crystals in it ?

Even the acetates conversion... wouldnt the fumarate and the acetate be fighting for the same spice ??

 

[endlessness]

As said, re-base it and re-extract. Both the fumaric acid (attached to the dmt fumarate) and the acetic acid (to the acetates) will be neutralized by the sodium carbonate and the dmt will become freebase, which you can pull with dry IPA/Acetone/Ethanol (or even naphtha/heptane, thhough I guess if you used limo in the first place, better avoid petrochems now too), so it doesnt matter that both fumaric acid and acetic acid were there.

 

[limoseen]

Ok in the end I couldnt be bothered re basing again.. so I evaped added some ipa and make some changa... was pretty splendid... good to know.. thanks for the advice endless and q21q21