too much saturated heptane? / low field (picture)

[Gardenic]

Hello.

It me again ( ͡° ͜ʖ ͡° )


I cooking MHRB (Cybs tek, but I think that everyone already knows about it)

Using 3 bottle at once.

I have only 200ml heptane so i thinking, maybe its be fine to use them with all 3 bottles.

I doing like This.

(4th bottle crash)

Now, after pour heptane from first bottle, to second, i have very saturated heptane.
Its fine? can i pour this to 3rd bottle?
i afraid, heptane doesnt pull any more (much saturated)

What do You think about it?

levels heptane are the same in 1st and 2nd bottle

 

[Gardenic]

nevermind.
Any way, its looks great 60ml per jar. used 150g mimoza.
How do You think? how much out?

 

[Tryptallmine]

Never heard of anyone saying saturated solvent is a bad thing around here....
Looks good, well done.

 

[Gardenic]

i Know, but i readed around here, 1 ml heptane can absorb something about 16mg dmt/fat/other stuff.
After second wash, heptane looks like milk, and I wondered, perhaps hep reached the limit of saturation.

 

[Tryptallmine]

i Know, but i readed around here, 1 ml heptane can absorb something about 16mg dmt/fat/other stuff.
After second wash, heptane looks like milk, and I wondered, perhaps hep reached the limit of saturation.

I would imagine that it'd actually hold more than that.

I've diluted 3500mg (3.5g) into 27ml of solvent before. It needed to be warm to hold that volume of alkaloids but it was possible.

If you think there might be more in your three jars. Wait until you've freeze precipitated your jars, collect the solvent and re-use it for another few pulls.

 

[Gardenic]

Done,
but, this time field is.. very low

I mix collected dmt with older crystals.

Little less than half of this, is from today.

MHRB can be after the date of expiry? mine have something about half years.

 

[cyb]

MHRB can be after the date of expiry? mine have something about half years.

MHRB will last for a long time (years)
Those milky pulls don't look right at all...
It appears that you messed up somewhere.

You really need to stick to the tek and not try and get creative...just do 50g and follow the instructions.

At least you got something :thumb_up:

 

[Gardenic]

I've done Your tek step by step.


I added only 51g Naoh instead of 50 to one of bottle.

I just had to do wash all 3 bottles with only 200ml heptane.

maybe i have to make pull one more time.


Edit: oh, i use kitchen salt, instead pure nacl. But in good quality

 

[3rdI]

keep pulling.

200ml isnt alot of solvent for 150g of bark

 

[chemicalg]

I'm going to do your tek in the near future cyb, I'm in the process of messing one up I think it's my 1st attempt, here's where I'm at thus far, A/B 250g acrb powder boiled in 1000ml water and 100ml vinegar x4 , my final reduction down to 750ml then filtered through a Büchner funnel which has produced a very light orange looking liquid of 500ml. I've added 100g of salt and topped back up to 700ml with distilled water . Now it's cooling till tomorrow . I started following an A/B tek by thick light and then I got wind of your salt tek so I thought I'd put some salt in. Now I'm totally confused and don't know if I've messed up as the soup was real dark before filtering and now it's a real light orange colour plus I added salt when I wasn't going too now I feel I'm hybrid teking. Wish I'd seen your tek earlier cyb. Any thoughts or input would be much appreciated

 

[cyb]

Any thoughts or input would be much appreciated

Just add salt at the basification stage (before or after) and carry on.
Salt can be added to A/B or STB or Hybrids.

See what you come up with...then (if you have 50g bark spare) do a separate run with the Hybrid ATB Salt tek and compare.

 

[chemicalg]

I kinda used it all during the boils but saved it all at the end and put into a container, would some if that work?, I've already added the salt I'm worried it's too soon as I won't be basifing for a while yet

 

[Gardenic]

keep pulling.

200ml isnt alot of solvent for 150g of bark

done, but nothing comes out

i really dont know whats going on. I "cooking" step by step;/

50-55g powdered MHRB
200ml de-water + 60ml de-vinegar
shaking 3 times (

after 1 hour

100ml de-water + 30g 99.9% jonized salt
200ml de-water + 50g Naoh
shaking 4 times

after 2 hours

add 50ml heptane
shaking for 30 secs. (mostly times foam appears)
pour heptane to jar
add 50ml (..) x4


maybe i shake too much? or too large/low temperatures? i always make sure the water was more or less all the time 55-60c