Consulting the 'glass shard pictorial' thread and faq, a recrystallization was performed on white powder obtained by gordo tek (modified q21q21 nn-dmt). Naptha was used, and after the heated solvent returned to room temperature there was absolutely no visible separation oils or mass at the bottom, instead nice looking crystals had adhered to the sides and bottom of the shotglass.
The rest of the naptha was decanted into another vessel, freeze precipitated then evaporated. The result of this was the exact same looking white powder that was introduced at the beginning. In the end what was left was 1/4 small clear crystal, and remainder being the white powder
Can anyone explain why these results were so much different than what its generally reported? Also what should be done to more effectively convert more of the batch in the future?
The rest of the naptha was decanted into another vessel, freeze precipitated then evaporated. The result of this was the exact same looking white powder that was introduced at the beginning. In the end what was left was 1/4 small clear crystal, and remainder being the white powder
Can anyone explain why these results were so much different than what its generally reported? Also what should be done to more effectively convert more of the batch in the future?
