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Use a pressure cooker??

CokFLHX

Esteemed member
Inwas looking around at how others grind or powder or thier bark. I just used a little magic bullet blender but it quit on me. Inwas looking for suggestions on a replacement and seen a mention of using a pressure cooker during the extraction.

I guess it helps to offset the bark not because my finely powdered and helps to extract all of the spice from the plant material.

Does anyone have any info n this or a tek in which it is spelled out clearly.
Or is it even benificial to use a PC?

From what I seen the PC was used during the acidification stage of an A/B. Said the bark In water with a pH of 4 was PC’ed at 15psi. I forget how long.

The temperatures reached under pressure of 15psi inside a pressure cooker can get up to around 250°F.

At what temperature does the DMT start to degrade?

Anyways….. any insight into this would be appreciated.

Thanks.
 
I use pressure cooker for most of my plant extracts... HOWEVER with rootbark atleast my lower quality bark I do not use anymore since it pulls over lots of fats/oils and forms a black tar which is a pain to deal with
 
pressure cooking can break down polymers and waxes that chemicals sometimes cannot reach, at least, supposedly, it does however also physically break down physical material that might be too tough for acid or base to penetrate, though ive never been clear on, wether its the PC time that does it, or, if its the cycling, people usually do 2-3 cycles for either 2 or 3 hours. its great if you are starting from whole bark or leaves.
One point of concern is not all PCs should cook with vinegar if they have aluminum parts, in which case you can just use citric acid instead.

Ive seen someone mention pressure cooking old bark they already extracted from and getting a huge yield, this was acacia however which doesnt play by the rules.
for MHRB i wouldnt bother if you can just grind and acid-bath it in the slow cooker for a day or 3.

lastly, freeze thawing and the use of a VERY strong acid like HCl can get the same lysolization and depolymerization effects eventually as well.
 
I found a way to really pulverize the bark. I mix that with a solution of RO water and HCI.

I’ve been doing three freeze thaw cycles of the acidic bark solution followed by an hour or so in a crock pot on high water bath.

You say the acid bark solution is no good with an aluminum PC? Even if the solution is inside a mason jar with a loosely fitted lid? I figured do it just like you would grain spawn, right?

But if the acidic bark solution would react with the aluminum pressure cooker even if kept inside its own jar I won’t try it.

I may just mix bark powder with RO water and PC that before I acidify.

Thanks for the replies and insight.
 
That’s what I figured…. Wanted to be absolutely sure.

Hey kind of a inrelated question…..

How do you guys measure pH? I’ve got the dippin’ strips but am almost out. Before I order more I wanted to see folks’ opinions on a pH meter pen. With the electrode you dip in whatever you want to measure.

Does anyone use one of these? Are they worth it? Don’t seem to be too terribly expensive. Pick one up from Amazon for around $30.

If anyone has any experience or knowledge in this area please weigh in
 
I don't measure pH. In most teks there's a significant excess of acid and base.

How much acid is actually needed to salt a gram of dmt?
 
Yeah. I kinda wondered if that was the case for most folks.

In one of the teks I’ve come across it specified adding more water/acid until the pH measured 3.

I would think that the goal is to get the pH to be less than or equal to 4 on acidify stage and greater than or equal to 12 when basifying and that’s really all you need, right?

Thanks again
 
That’s what I figured…. Wanted to be absolutely sure.

Hey kind of a inrelated question…..

How do you guys measure pH? I’ve got the dippin’ strips but am almost out. Before I order more I wanted to see folks’ opinions on a pH meter pen. With the electrode you dip in whatever you want to measure.

Does anyone use one of these? Are they worth it? Don’t seem to be too terribly expensive. Pick one up from Amazon for around $30.

If anyone has any experience or knowledge in this area please weigh in
ph doesnt change much when diluted, if salt content is an issue, take samples and dilute by 20x, or, experiment with your chosen acid to see where the curve is. pH is logarithmic, off hand i dont know how it converts to real quantities but if you have a solution of ph4 acidic water, not including actual reactions that are occuring that result in no change to the H+ concentration, it would take 100x less acid to give you pH 5, and 100x more to give you pH 3
also, another thing to consider is that the dilution factor becomes much less significant the further you are from neutral.
Lastly, consider getting pH standards and calibrating with those, or just have them handy as a refference to check for drift, using ones already close to some of the more gentle setpoints you intend to use. measuring things like pH 6 or pH 8-9 are where things get tricky. but your proble should pretty easily distinguish 9 from 14 or 4 from 1
to that end, a simple $5 one sold for beer is fine, again just keep standards handy to test for drift.

extra last- i used to work in a lab and do maintenance and calibration on pH sensors that cost like $20K just for the probe itself.
even good sensors will drift over time. i dont know the exact mechanism but its kind of like the ionic forces need to equalize through the bulb or something, and the sensor, or its circuitry, responds very well when theres a big difference in the in/out.
As an example, if i just exposed the probe to cleaning solution its reading 14, i rinse heavily with tap water, then distilled water to remove tap water, then i put it in a pH 7 calibration standard, it quickly shoots down from possibly 10 at that point, to 7.5, and over 10 minutes settles at 7.
20m later it could be anywhere from 7.2 to 6.8 and going all over the place. cheaper probes can drift in a buffer by up to 1 whole pH unit.
So when testing with cheaper probes who are worse with the drift that, the smaller the difference its trying to test between what it says it is currently, vs what is outside affecting it, the worse its accuracy becomes. its like draining water through a pinhole. the less water is left the slower it leaks. So get good at presumptive reading, observe where its going, not where it lands. fancier probes use integration math to calculate where its going to land and then locks the value in to there once it slows down enough. If you have done/remember calculus, this is one of those things where in integration you end up with an impossible answer because it approaches zero or some value, like, using the rectangles under the curve visualization method. In the case of the pH probe once the difference between the probes internal pH and the external pH is like 1%, the signal gets amplified in a distorted way or it just totally loses track altogether, kind of like loud tinnitus if you are in a room thats too quiet.
otherwise it may never stabilize at mild conditions. Hard rule is probably, try and get your reading within 3 minutes tops, and rinse the sensor with deionized/distilled water right before use.

Ernestine said:
How much acid is actually needed to salt a gram of dmt?
theres no fixed answer. pure DMT requires stoichiometric amounts, probably. DMT in bark is surrounded by other substances like tannins or minerals which function as buffers, where you can add acid or base and it reacts with the tannin/tannate resulting in no change in pH until all of it reacts. known predictable sources are why some teks can just say use X amount of ph4 water or whatever. alternatively, they massively overshoot and deal with seperation much later, but i found thats not practical for acacia.

When i was dealing with maidenii, i found it was best to titrate a small sample as maidenii contained stuff that would form an unfilterable gel if overshot, so about 4x i tried it in a test tube to find out how much it took to basify, then i added 80% of that to the main liquid and very slowly did the remaining 20%, which was far easier than doing it blindly. plus stuff crashed out which could be eliminated
 
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