So after a few failed attempts I finally pulled crystals from a small STB extract of Acacia Confusa. I only used 50 grams of powdered bark and already got a bit of clear goo from the first pull. I did keep the DMT rich Naphtha though to see if I could figure out how to crystallize it and finally got a small amount from the first pull. There probably would have a significant amount more had I thought of this the first time, but it's a progressive step nonetheless!
I just let my jar of solvent and goodies sit in the freezer overnight again then today noticed the jar had the expected layer of gooey crystals (which is probably where most of the DMT is) and quite a few floaters in the party. So I decided to pour it through a coffee filter, hoping to allow the crystals to dry without any goo coming with. It worked! Only have about 40 mg of crystal since this is the same first pull I've been working on for about a week, but I kept the solvent I poured off and put it back in the freezer to see what else comes out.
I'm just pleased I finally made a step towards figuring out crystallization doing an STB ex on ACRB..
I just let my jar of solvent and goodies sit in the freezer overnight again then today noticed the jar had the expected layer of gooey crystals (which is probably where most of the DMT is) and quite a few floaters in the party. So I decided to pour it through a coffee filter, hoping to allow the crystals to dry without any goo coming with. It worked! Only have about 40 mg of crystal since this is the same first pull I've been working on for about a week, but I kept the solvent I poured off and put it back in the freezer to see what else comes out.
I'm just pleased I finally made a step towards figuring out crystallization doing an STB ex on ACRB..

