So I have a nice new stir plate and I notice that while using it the basified solution can be gently swirled underneath the NP without being thoroughly mixed up and emulsions can be completely avoided. My question is. Does mescaline 'migrate' into the NP? The stir plate turns the bottom layer over enough so that it all comes in contact with the NP and this leaves the non polar lovely and clear... I was unsure and impatient so I ended up thoroughly mixing it and consquently I'm now sitting over a hot water bath clearing an emulsion. Perhaps this can be avoided in the future?
