Anyone have an easy Chaliponga TEK?

[Fungaai]

Hi Nexians!

Anyone have an easy chali tek? Lextek has been suggested elsewhere. Also, once the extraction is done, how does one seperate the 5-meo and the N-N-DMT?

Thanks!

 

[dreamer042]

iso tek for chaliponga/leaf sources

Is there 5-MeO-DMT in Diplopterys Cabrerana / Chaliponga?

 

[Infundibulum]

STB also works fine with chaliponga.

 

[Fungaai]

STB with the leaf? I've tried that and it's didn't work.

 

[Infundibulum]

STB with the leaf? I've tried that and it's didn't work.

Weird- do you mind describing your method? What exactly did not work and how did you assess failure?

I've done STB in chaliponga in a few times in the past, with success. I've pulled with naphtha as well as xylene.

 

[Fungaai]

I used xylene. Don't know if I have the PH right though. I used 37.5g of NAOH in 500ml water. Don't know if that's too much.

 

[Fungaai]

If the yellowish green goo end product indicates success. How does one clean it up? I hot naphtha, but all of it dissolves.

 

[Infundibulum]

You've got to be more descriptive, also see this tread for more instructions.

As you realise, it is hard to get helpful feedback if you do not describe your process thoroughly. How much material did you use, dissolved in how much water, what did you do after you collected your xylene pull etc etc....

 

[Fungaai]

Okeydokey...

500ml water with 37.5g of NAOH dissolved.
Shaken and stood for an hour.
Added 50ml of xylene and shaken intermittently for 12 hours
Added 50ml of xylene and shaken intermittently for 12 hours
wait for seperation
Siphon of xylene
Repeat above steps
Combine xylene and evap.
The end result is a yellowish-green syrup.
Then a naphtha recrystallization was attempted assuming the DMT would be taken into the solvent and everything else would stay behind.
All the syrup was dissolved in the solvent instead.

Any ideas?

 

[Apoc]

standard a/b works fine. boil leaves, reduce if you want. base it, solvent it, fasa it, then convert to freebase with sodium carb, or just leave it as fumarate.