TEK Converting CBD to THC using only Zeolite and heat.

[15082130]

Hello dear forum members!
I have a question. As i've heard the delta-9-thc is the kinetic byproduct of isomerisation and delta-8-thc is a thermodynamic so for better d9 yield it's better to perform reaction with less time and higher temperature. So here's the question: has anyone tried to quickly cool the mixture immediately right after synthesis to stop the reaction of isomerisation of d9 to d8? Because i think cooling our mixture after synthesis simply by waiting creates a place for unwanted reactions of isomerisation of d9.
English is not my first language so if there are some mistakes im sorry. Thank you.

EDIT: Also everyone here is preheating to 105 and then increasing temperature to 150. What if i preheat to 135 and wont change the temperature for better consistency of reaction?

 

[imeatall]

Hello dear forum members!
I have a question. As i've heard the delta-9-thc is the kinetic byproduct of isomerisation and delta-8-thc is a thermodynamic so for better d9 yield it's better to perform reaction with less time and higher temperature. So here's the question: has anyone tried to quickly cool the mixture immediately right after synthesis to stop the reaction of isomerisation of d9 to d8? Because i think cooling our mixture after synthesis simply by waiting creates a place for unwanted reactions of isomerisation of d9.
English is not my first language so if there are some mistakes im sorry. Thank you.

EDIT: Also everyone here is preheating to 105 and then increasing temperature to 150. What if i preheat to 135 and wont change the temperature for better consistency of reaction?

hi bro! We haven't come to a single method, but here's what I've heard: 7 minutes, 2 Zeo:1 CBD, 150°C, produces a Delta9 effect for many people, although this mixture retains most of the CBD. Someone wrote that 120°C is the most favorable temperature for D9. Two people did this. One used 120°C for 40-80 minutes, 2 Zeo:1 CBD. The other used 4-5 Zeo:1 CBD, 120°C, 10 minutes. He said the effect was similar to D9, and that more than 100 mg gave him a bad trip. I'm inclined to think the issue is bioavailability. I think you should try both 120°C and 150°C. Apparently, in the first minutes of the reaction, we get pure D9/CBD, and after a while, D9 begins to convert to D8, with D9 ceasing to appear during the reaction.

 

[15082130]

hi bro! We haven't come to a single method, but here's what I've heard: 7 minutes, 2 Zeo:1 CBD, 150°C, produces a Delta9 effect for many people, although this mixture retains most of the CBD. Someone wrote that 120°C is the most favorable temperature for D9. Two people did this. One used 120°C for 40-80 minutes, 2 Zeo:1 CBD. The other used 4-5 Zeo:1 CBD, 120°C, 10 minutes. He said the effect was similar to D9, and that more than 100 mg gave him a bad trip. I'm inclined to think the issue is bioavailability. I think you should try both 120°C and 150°C. Apparently, in the first minutes of the reaction, we get pure D9/CBD, and after a while, D9 begins to convert to D8, with D9 ceasing to appear during the reaction.

Thank you!
Also what if we try to increase the acidity of zeolite by adding small amounts of citric acid and some ascorbic acid for antioxidant properties? I've read almost everything available about this method on forums that i got my hands on and heard this might work. Also I believe that increasing the surface of reaction mixture will be better for controlling our reaction and better for it consistency. I will try to make two batches using 0.75g of cbd + 1.125 g of zeolite and ~0.1g of citric acid on pan. I'll post my results here stay tuned!