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Dmt not precipitating out of naphtha in freezer.

Migrated topic.

crakkbakk

Rising Star
Stb with 100g powder rootbark, 100g NaOH. Base was black and was combined with rootbark for 6+ hours.
150mL added, rolled. Sat for 24 hours. Naphtha pulled off placed in freezer for 24 hours.

Jar looked white but it was probally just frost... Shaken up a bit, poured through filter. Nothing on the filter, nothing on the jar it came out of.

Is it possible the slight shaking dissolved the majority of the dmt back into the naphtha and the coffee filter was too big and let it all slip through?

Naphtha added back to mother jar with rootbark water and NaOH.

What went wrong?

Plan to get super thin filters and not shake up naphtha tomarro.
 
it seems like you possibly just had too much naptha and the solution wasn't saturated enough to allow for precipitation.

reduce the total volume of naptha by 50% and re-try your freeze precip.

I could be wrong, but it seems likely.
 
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