DoorSeeker
Rising Star
Does anyone know whether it is valuable to evaporate down your naphtha before freezing when doing a recrystallization? I think theory would answer this question. How much dmt can naphtha hold when at something like 0 degrees F? I see huge ranges for how much naphtha to use for a recrystallization. Everything from just enough drops to dissolve everything (which can easily be just a few ml per gram of dmt) to 50 ml per gram. Here's the real question, if I did recrystallizaton at 5ml per gram of dmt or 50 ml per gram of dmt would the difference be negligible? I'm trying to figure this out because if you use too little you are leaving a decent amount of dmt behind because the small amount left over to keep from pouring out the gunk at the bottom is still highly concentrated but if you use too much you risk not having all the dmt precipitate out... well maybe. That's what I'm trying to figure out.
If anyone knows how much dmt naphtha holds at freezing this should answer the question. I've seen the numbers before but I can't seem to find them again. Thanks.
If anyone knows how much dmt naphtha holds at freezing this should answer the question. I've seen the numbers before but I can't seem to find them again. Thanks.