LSA recristalization? + Storage

[Smoker root]

Hi I made a extraction from a Lot of HBWR seeds using a simple tek that gives a yield high enough to use the LSA to make LSD(but se abre not talking about that today) It basically deffats with NAFTA, extract with cloroform amonium hydroxide, tartaric acid and finally extracts everithing with clorofrom (I would probably post the Tek) I have to note that it yielded cristals

Which is the problem? That this seeds creates other molecules similars to LSA that are usually soluble in the same solvents that is why, Aldo it is basically unecesary , I want to recristalize. Any good solvent?

I was also asking a long way of storing the LSA I think a good idea is to Jeep it in a solution of cloroform with some ethanol to prevent fosgene production, ir just store it as LSD

Thanks you, love you all

 

[sbc1]

You should write up a tek and post it

 

[DreadedShaman]

I mean... If you know how to start with LSA and end up with LSD, why wouldn't you just make LSD? I'd think LSD is more desirable than LSA

 

[Brennendes Wasser]

For storage I would just place it in Ethanol with a little of anti-oxidans like fumaric acid or vitamin c or melaton even maybe? Otherwise pure Ethanol (94 %) was also still good enough I think ...


What is the yield on the seeds? I remember that Kash's TEK (the most prominent at Nexus I think) had very low yields ... But even if you have a yield, are you even sure that it is pure LSA? Should matter for the yield calculation ;O

 

[Smoker root]

For storage I would just place it in Ethanol with a little of anti-oxidans like fumaric acid or vitamin c or melaton even maybe? Otherwise pure Ethanol (94 %) was also still good enough I think ...


What is the yield on the seeds? I remember that Kash's TEK (the most prominent at Nexus I think) had very low yields ... But even if you have a yield, are you even sure that it is pure LSA? Should matter for the yield calculation ;O

That is what I am worried about. It is a method that it has been múltiple times tested and it gives some Nice results, but I am not sure it is pure LSA(that is why i look forward a recristalization) However, it is pure enough to use ir as a precursor for LSD-25 so I think it is really puré. And at least I can see that it extracts all, if not most of the alkaloids(fue to fluerescens under black light)

 

[Smoker root]

I mean... If you know how to start with LSA and end up with LSD, why wouldn't you just make LSD? I'd think LSD is more desirable than LSA

LSA is used as a precursor and LSD requires a great knowledge, of course the synthesis is un theory easy. But you have to do it under nitrogen atmosfere, with no water, with no UV light, and being carefull not yo come un cobtact with any of your product because it could fuck you up.

That is why I prefer LSA