My Fifth MHRB A/B Extraction (Went Awesomely)

[hostilis]

250 G of Brazillian MHRB A/B Extraction.

Ingredients
• Vinegar
• Distilled Water
• Vinegar/Distilled Water 1/3
• Sodium Hydroxide
• VM&P Naptha
• Brazilian MHRB


Procedures

I. Acid Washes
• The first acid wash
(1) I used 3 liters of 1/3 Venegar/Dist. Water And boiled for two hours.
(2) Then I let it decant on a cold burner for about 10 minutes
(3) Then I pour through a wire mesh spaghetti strainer into another container
(4) Then Strain it through a funnel and piece of cotton rag
(5) Strain through a coffee filter.
• The Second Acid Wash (repeat first one)
• The Third Acid Wash (repeat first one)
• The Fourth Acid Wash
(1) I used 5 liters of 1/3 Venegar/Dist. Water And boiled for five hours.
(2) Then I let it decant on a cold burner for about 10-15 Min.
(3) Pour through a wire mesh spaghetti Strainer into another container.
(4) Pour it through the cotton rag in a funnel
(5) Strain through a coffee filter
• Rinsed the MHRB with distilled water to get the remaining DMT Acetate out.

II. Evaporating Excess and Filtration

• I mix all of the washes and put them into a big pot and boil it down to 400ml
• Let that mixture decant overnight in the refrigerator.
• Filter that mixture again through a coffee filter using a funnel and beaker.

III. Basification and pulls

• Using sodium hydroxide, basify the mixture to a ph of 14
• Naptha pulls
(1) Mix the basified mimosa soup with 15ml of naptha
(2) Stir it with a glass stiring rod for about 5 minutes.
(3) Pour into a separatory funnel and let it separate
(4) Pour off the bottom layer and put it back into the mixture beaker
(5) Pour the naptha layer into a clean, wide mouthed beaker and save.
(6) Repeat steps 1-5 four more times and save the naptha layers.

IV. Freeze precipitation

• Make sure the DMT containing naptha does not have any basified mimosa soup in it
• Place the beaker in a very cold freezer and let it sit for 12 hours (overnight)
• Once that is done then pour off the naptha through a filter to catch any crystals, and scrape out the precipitated DMT
• Chop it up and let it dry out.


This Extraction went extremely well. I got 2.7g of DMT in the final result. I feel that it went very well and the final yield was a little bit over 1%. The product was white and sparkly and smoked very smoothly. It was my fifth A/B extraction and the best yeild and most consistent, nice colored, product i have ever gotten. I am starting to understand this a lot more. I went on a very nice journey with this stuff . And many more to come. The picture below is just a small amount of it and is pretty blury, but it is the only one i have.

 

[zombicyckel]

That look very nice!

 

[Rivea]

Good job. It looks good. There is probably nothing left in that bark after the 5 liter boil at the end.....

 

[hostilis]

Yeah, for sure. It was a good yield and clean product.

 

[Pandora]

That looks great and that yield is nothing to be ashamed of.

 

[hostilis]

It was great yield for me! I have only been getting .5% usually out of it.

 

[LRx]

This is AWESOME!
Good work, hostilis! :thumb_up:

 

[The Day Tripper]

Very good technique.

I particularly like how you reduced the tea to a small volume, used vinegar/distilled water, and only a small amount of naptha was required due to the concentration of your pulls. I'd keep pulling with fresh naptha/a heat bath and see if you can coax any more dmt out. Should really increase the solubulity of the dmt in the naptha, and help in separation of the layers.

Props for your frugality in extraction supplies, by reducing your initial acid pulls heavily, before basing/np pulling. So much more efficient than stb's, or acid bases that don't reduce the liquid down to less than 500ml per 250g of bark or so. I just reduce until it starts to get thick, then add enough distilled water to make it almost as viscous as water, but no more.

I remember back in the day when people used 100's of grams of lye, liters of water, and hundreds of mls of naptha to extract. A heat bath, a fraction of that scale, and proper decanting/filtering give the same results using so much less solvent/base.

 

[adam]

I like this tek, I will definitely be using it soon.

Would be cool if you added pictures:thumb_up:

 

[darellmatt]

Nice work. I will definitely be using your methods next time I extract!