Possible to use D limonene on material after Naptha?

[93bywayofthedear]

As I mentioned in my first post, I did my first extraction of 200 grams of Mimosa and received a little over a gram of fluffy white crystals. I used the q21q21 Vinegar/Lime_A/B_Extraction_Tek After 4 pulls with naptha, I let the bark material dry out completely and saved it for some reason. After reading more about extraction teks, I began to wonder if there was a way to extract jim jam from the same bark with D-Limonene? If so, what would be my next steps.

Thank you

 

[justine]

Well yes you can definitely pull with D-limo, especially since your yield was quite low (and so there is probably a lot of dmt n-oxide in your bark).
If you've let the basified bark material dry out you can try a d-limo dry-pull, otherwise add water, check the ph and pull just like with naphta.
Once you have pulled with d-limo you have to salt with fumaric acid, check the wiki for more informations!

 

[Eden]

Absolutely.

Not sure if a dry pull would work well....you will likely lose some limo in saturating the bark mix.
Just add water to restore the sludge as justine mentioned and repeat the q21q21 tek with limo instead of naphtha, maybe adding additional lime for this second run.
If you don't have fumaric available, you can salt out with vinegar instead for some lovely jungle acetate. With your current yield, you should get a nice surprise.

 

[93bywayofthedear]

Thank you so much for the reply Eden and Justine.

 

[93bywayofthedear]

Hello, I followed the directions on the same tek using limonene instead of naptha this time. I added enough water to make the bark wet throughout and shook in a bit more lime for good measure since I do not have a ph tester. I hope that worked.

I made three pulls on the 200 grams of rootbark and salted out with vinegar. I believe I used too much vinegar. I now have about 125 mil of yellowish colored dmt acetate in a 200 mil wide mouth jar. It is my intention to use the finish product for infusing with some enhanced leaf. I already have a yield of white crystals that I intend to use for freebase, so I am hoping now to produce some "Jim Jam". This is something I would like to experience.

I have done quite a bit of reading and I am still a bit unsure about the process of using heat to evap my jar of liquid.

I have two questions.

My first question is about the tempurature of this procedure. I have read that Jim Jam should not be heated over much more than 100-125f or so. But if the liquid in my jar is mostly water and vinegar at the moment, might I introduce it to a higher heat until most of the water and vinegar are evaporated. I am going on my understanding that dmt should be able to handle boiling temperatures in aqueous state.

My second question is regarding the method. I was hoping to just stick the open jar in the crock pot on high, let the vinegar, water boil off a while and then after it gets mostly evaporated, I could turn it on low and set it on a peice of cardboard to protect it from direct heat of the element and keep a close eye on it until it is done?

Any suggestions will be appreciated. Also My heart is not set on any particular method. It is simply to get from point a to b without making a rookie mistake.