Nope, they do not evep away like hcl. In these cases the solvent mix (and excess acid) was decanted or filtered off leaving only pure crystals. The starting material was tan mesc hcl that had been washed in MEK already, so no cleaning was needed.
Kash said:Added 100ml h2o to combined toluene extracts and set to stir.
Stir plates are amazing. But ya only need to do one salting of the total toluene via a titration process that dg sums up nicely in another thread, nice and hassle free.cyantific said:Kash said:Added 100ml h2o to combined toluene extracts and set to stir.
Did foaf salt the toluene pulls with just 100ml of water? Or did he do multiple saltings?
Clever use of a stir plate.
Kash said:Good luck 3rdI, hope it goes well.![]()
