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SAFE d-Limonene+calcium hydroxide Tek?

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hey syzy, nice to see you're still around :)

one question: how much water is used when mixing the acetic goo with sodium carbonate? Only enough to make a paste, or a bit more so that it becomes a solution ?

and also, what kind of container does SWIY do this in? I ask because I was wondering how for getting the acetic goo, it would be evaporated from the vinegar pulls, and for evaporating one usually makes in a wide low container.. but then to make this water+freebasing and iso+separation, it sounds like the kind of thing that would be better made in a taller and thinner container so that the separation is easier.. But then how to transfer the goo from wide container to another? And the separation of the iso, pippete is the way, or ? Or what other suggestion can you give regarding the practical aspects ?

SWIM is finally very close to experimenting with this tek, as he found limonene and IPA where he is living! Thanks for the help :)
 
Has anyone tried cold precipitating dmt crystals out of the limonene in the freezer?

Any reason why that wouldn't work?
 
^
Not personally, but SWIM has read from multiple sources that it does not work, not sure why though. Presumably because it has a high boiling point, freezer temperatures are not enough to cause the d-limonene molecules to contract enough to crash out the DMT. Or maybe it's polarity makes it to where it's only possible to separate through chemical reaction, ie salting out with acids. Can anyone explain why, now SWIM is curious?
 
can anyone tell swim if once freebased from acetate, the resulting alks will dissolve into acetone? Is that a good route to enhanced leaf?

iso is restricted where SWIM lives and he can't get it

so its either use limo or use acetone, if all the freebases are soluble in acetone he will use that because he uses it to clean mesc and it leaves no residue
 
Since it's now known that mescaline acetate is insoluble in MEK, would it be true for DMT acetate as well? Could non-pure DMT acetate be separated from the other alks with cold MEK as well?
 
Noob said:
Since it's now known that mescaline acetate is insoluble in MEK, would it be true for DMT acetate as well? Could non-pure DMT acetate be separated from the other alks with cold MEK as well?
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SWIM was interested in the answer to this as well
 
mapp said:
Noob said:
Since it's now known that mescaline acetate is insoluble in MEK, would it be true for DMT acetate as well? Could non-pure DMT acetate be separated from the other alks with cold MEK as well?
Click to expand...
SWIM was interested in the answer to this as well
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Well when salting out DMT from limonene/xylene the product produces STRONG near-breakthrough effects at 15-20mg and breakthrough at 25-30mg for SWIM. So there really is no need to purify it further. This of course using heat to freebase and smoke as seen in Q21Q21's tek.

That is using lime to basify the MHRB though, the excess PH from lye may product different result.
 
Anyone have a more clear answer?

Edit: Sorry, is Swiy saying "yes"?. Also, Swim is curious how he would go about getting jimjam or jungle spice with this tek? Would that be in the MEK? Or would he do something different with the d-limo instead of salting with vinegar?
 
a couple of things


1. acetate is smokable, it freebases with heat, consequently instead of your usual number of hits, take one more
2. goo hardens as it dries, use a dessicant or get better evapping skills
3. dlimo>other nps for safety and pulling power

the red goo is my favorite, it reminds me of the incomplete philosopher stones from full metal alchemist
 
Ash said:
Is there a more detailed thread of this tek? I can't seem to get the limonene to mix with the mimosa. It just stays at the top so I'm not sure if it passed through to pick up the spice :/
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having the same issue, limonene doesnt pass through. Any suggestions ?
 
the limonene is supposed to sit on top.
this is good.

i like to stir mine (make sure you have a material that won't be degraded by the limo) vigorously.

there is a noticeable color change after a proper stir (generally my limo goes from clear to yellow when it sits on the bark, and from yellow to orange/red after a vigorous stir)
 
endlessness said:
sounds wonderful! if only SWIM could find limonene

?
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Have you tried art supply stores? Theres one here, and I think its national (US) that rhymes with "dick" that carries a brush cleaner that lists d-limo and l-limo(?I think- something like that) and I think thats all. Havent looked up the MSDS as Ive not used it. Its spensy, like $10 for a small bottle. Its called natural-cleen or something. Sorry to be so vague, but you can find it, I'm confident in your cognitive abilities.
 
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