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wierd layers

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ucorky

Rising Star
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ok. Swim's got an issue. Extractions have been done (STB mainly), and dried in dishes and beakers. With all the various experiements dried, gooed, scraped and so on, he decided to dry it all out down to solid, and redissolve it all in a beaker of plain water, bassify it, then add d-lim to it. Its a thick mucky spoiled milk consistency with all extractions combined. The xtractions have been a summer project.None of this stuff was done in any rush.

The result was an immediate beaker of what looked like spoiled milk with a layer of d-lim on top. After a while layers formed in the following way. A bottom layer of what looks like slightly dirty undissolved salt, a layer above that of rusty water, then next (still going upwards) a thick layer of spoiled milk sort of looking gurgle, then a clear layer of D-lim.

I know this IS something significant. Please reply.
 

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correct. I left it all basified and in fact kicked in some extra lye to make sure it was so.
I really want to just take it all, evap it all, then do this over.

I know the picks arent very good.

Today SMIM has taken some Naptha soaked material and dumped it in with d-limo soaked material. Nothing is really happening in
the d-limo beaker anyway so he figured 'what the hell'. The curdled milk-looking stuff is floating between the brown and clear layers. Not on top of it ALL or the very bottom either. Some sandy looking stuff is on the bottom.
 
im sorry you're not making much sense to me. DMT shouldnt dissolve in water and specially basified water in the first place. Are you sure you saw freebase dmt dissolve completely in basic water?

And the rest of the explanation is very strange. What is "naphtha/limo soaked material", is it literally naphtha/limo with something dissolved, or is it a solid product (freebase dmt?) ?

Try to make clearer step-by-step explanation of what you did. For example:

1-I mixed x amount of substance with y
2-I stirred until it most dissolved but some remained undissolved
3-After 10 minutes the color changed

(or whatever, but please clearer or it will be impossible to help you)
 
I can defintely say I didnt dissolved anything in water other than the waxy part. All this pouring back and forth in various solvensts and water if anything, has increased the amount
of the pond scummy looking stuff floating around. Maybe this is the product I am seeking. Amounts and all that, has been all summer long, so I'll need to readdress it all. I guess I am just not chemically oriented enough to ask.
 
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