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Expected loss after soda wash?

Back2Normal

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I redissolved 4 dry grams and washed it, ended up with 2.75 dry afterwards. Solvent looked super clean before the freeze precipitation and during wash, didnt see junk in it really. I understand now that I got rid of some red polymerized dmt, thinking that it was plant oil and not dmt. But I was just wondering if there is an expected percentage of loss when redissolving. Is some of it just still trapped in the solvent I decanted off before drying the crystals?
 
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