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extraction

  1. T

    DMT ethanol extraction from DMT & calcium hydroxide slurry.

    Someone suggested that basifying a crude xylene extraction with Ca(OH)2 and drying it would allow one to extract the DMT freebase from the slurry, leaving behind the Ca(OH)2 and calcium acetate (having used acetic acid for the aquesous phase) as they are not soluble in ethanol. Now, what's...
  2. T

    N-oxide solubility in water and DMT from DMT-N-oxide separation with H2O

    On thttps://wiki.dmt-nexus.me/Psychedelic_Compounds_Chemical_and_Physical_Properties#DMT_N-Oxide "...Soluble in water..." without further info is stated. If someone had obtained a "full spectrum" extraction with xylene containing DMT and its N-oxide, could plain distillied water be used for...
  3. Self-container

    Mask(s) for DMT extraction

    I have found two threads on this matter already, though the links provided were dead. As far as content go, they simply mention that one needs a P3 mask, which is a mask that has the highest safety rating. As such, a P3 mask can be many different things. Although a mask with a P3 rating does...
  4. Self-container

    Techniques for evaporation

    I have never extracted DMT before, and whenever I read TEKs, I find myself most hung-up on the evaporation step (if applicable). I wonder how to do it, practically. First of all, I wonder what temperature to have; though that would depend on the non-polar solvent used, so I guess I can just...
  5. S

    Better STB

    So I read the Lazymans Tek and saw that he had gotten 1g out of a Lb of rootbark his first pull which is way to little. Try this. Put 2Kg powdered root bark in bucket, Add three pounds lye and a gallon of water, Stir 3 to 5 min the high amount of lye will cause the water to get extremely hot and...
  6. T

    Is there a limit to reducing (concentrating) acid pulls from MHRB?

    Is there any limit to how concentrated one could get the acid pulls from MHRB? I suppose the lower the volume, the easiest it should be to actually pull the compounds of interest with non-polar solvent after basifying, but is there a maximum level of thickness/viscosity I should stay clear of?
  7. Re-x-ed with acetone

    Re-x-ed with acetone

    The most neon yellow DMT I ever extracted. Probably lots of Oligomer going on since I heated the solution to 65C on my hotplate stirring bar. With the knowledge from the thread from Loveall I will not do that again. 26C max heating with silvent solvent on top (that has a boiling point of only 32C.
  8. pete666

    STB Mescaline Extraction TEK

    Main purpose of this TEK is to have emulsion-free procedure which leads from cactus matter to pure white mescaline when followed properly. This TEK is based on this topic describing emulsion-free procedure for initial extraction and adds salting/titration and further purification. So now it can...
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