JamseyBoy23
Rising Star
Need some advice on what whether or not if it's necessary to do both a wash and a recrystallization also does this extracted naptha look SOAKED or what? Looks like lemonade makes my mouth water 
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A/b questions on re-crystalization and purification
- Thread starter JamseyBoy23
- Start date
context is required.
it looks like its gone cloudy-milky after being frozen. if so, thats not a problem, provided you are using naptha.
otherwise you could have a horrific emulsion there, or just simple calcium contamination.
shaking it with saturated brine might resolve this, the brine afterwards is easily pipetted away. sodium sulfate or other dessicants can be beneficial, they do wonders for makinng things go dry and clear. and dry naptha will crystalize infinitely better than wet
it looks like its gone cloudy-milky after being frozen. if so, thats not a problem, provided you are using naptha.
otherwise you could have a horrific emulsion there, or just simple calcium contamination.
shaking it with saturated brine might resolve this, the brine afterwards is easily pipetted away. sodium sulfate or other dessicants can be beneficial, they do wonders for makinng things go dry and clear. and dry naptha will crystalize infinitely better than wet
The blue fluorescence is at least a positive sign. This appears to indicate you have a fine suspension of DMT. Stick it back in the freezer for another day or so, maybe it will resolve into larger crystals.
But really, we could do with just a tad more info about how you got to where you are now with regards to this extraction.
But really, we could do with just a tad more info about how you got to where you are now with regards to this extraction.
