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D-limonene Tek and 99%IPA?

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Geines

Rising Star
Question is below, ignore the first part if you want.

(How I did the d-limonene tek: I followed Ron69s method using 150gs mhrb blender shredded, even though I used the exact amount of water, he noted it shouldn't be watery and it was indeed watery. So I evaporated some of the water in an oven until it was damp, no excess water was visible. Added the limonene which turned brown, I think instantly, mixed for 5-10 minutes and following some advice left it for a day. D-limo's all brown poured it off, added vinegar (twice as much because the D-limo was brown and the vinegar was brown and I needed to see a clear separation), mixed and waited, saw bark particles so filtered again and again, chose to experiment and evaporate D-limo with vinegar, note D-limoonene is not edible in fact it's moderately toxic says the health and safety data sheets online. I think that data should be posted in the tek since technically D-limonene isn't food safe. So I evaporated the mix in an oven at 50c until it was a brown goo.)
(I dosed the goo for Ayahuasca and had a bad reaction, throat almost closed up which I attribute to the d-limonene. Thinking about it, there should have been very little D-limonene in that goo if any at all since it did separate from the vinegar and turned back into a yellow liquid, and most if not all did evaporate. The reaction then could have come from the vinegar. I took 13g of that goo after 4g of syrian rue seeds. But no dmt effects where felt. Also I have mixed 5g of goo in a glass of vinegar and have yet to see a d-limonene separation.)
EDITED

So I got the D-limonene vinegar mix brown goo, 5-10g, and put it in a small jar and filled it 3/5 with IPA. I was hoping a separation would occur and it has. I'm not exactly sure how much D-limo is in that goo. So the top layer is near clear yellowish liquid, below is a more thick looking layer which starts yellow then quickly turns brown. So I was wondering if dmt is soluble in IPA from dmt acetate and if could use the clear liquid for changa. Or similarly what happens when you mix IPA or acetone with dmt acetae?
 
Geines don't worry about failing. I think my first two extractions were at total disaster and I'm still learning... It takes some practice and some understanding to get it right, also the right tools and chemicals are important. I'm sure you'll get it right eventually. I would try to follow one of the easier teks with a workable amount - like 80-100g of mimosa powder.

I would suggest Jorkest tek but if you can't find lye then I guess Q21Q21's tek should work as well. Personally I also like working with naphtha more than limo because you can freeze precipitate and don't have to go through the salting procedure. But working with fumaric acid saturated IPA (FASI) to salt out the dmt from the limo works too... you just might have to clean it a little and then if you want to smoke it convert it to free-base, for which the wiki has some neat instructions.

If you need some quick online help you can always join the chat, thats what got me through my extractions in the beginning :p
 
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