On any medications?
No dude, I didn't use medications or psychedelics. I didn't even use marijuana.On any medications?
I'm sorry but I don't think this is mescaline.
I rinsed it with a little ethyl acetate. Then I dried it. This looks more like lime than anything else. I tasted it and ;
It tasted like calcium oxide , and so did its appearance.
I dropped 5g in 1.2L of EA without stirring and at the end I found citric acid not dissolved when i scratched the xtals (it was under a coat of mescaline citrate). What would be the best ratio (citric acid/EA volume) to have exces acid totaly dissolved ?Wiki said:Drop ~5 grams (~1 teaspoon) of citric acid into extract. ... . Allow the citric acid to dissolve by diffusion without stirring. ... . If the citric acid is anhydrous and/or coarse it may take a while to dissolve, however it WILL dissolve fully
Firstly, I'm not in Oz, so take that as a disclaimer from the outset!Hey,
I don't live in the US, and I am having a hard time finding: Ethyl Acetate and Citric Acid.
I went to any hardware store around and wasn't able to find those.
Where are they usually sold?
Do they go by any other name?
Is there any replacements I can use to perform CIELO method?
Thank you!Firstly, I'm not in Oz, so take that as a disclaimer from the outset!
Citric acid is a culinary ingredient that can often be found in middle eastern type grocers, and it may or may not be available in domestic supply stores as a descaling agent. It was quite hard to find in the UK for a time, apparently to discourage the heroin addicts
Ethyl acetate may be available from specialist plumbing suppliers as a pipe welding solvent for PS waste pipes, where it gets dubbed as "MEK substitute" (in N America, at least). A similar solvent to look out for is butyl acetate, which appears to work for its own version of CIELO (therefore, "CIBLO") but the crystallisation step with the citric acid may well require some refinements, since the solubility of both water and citric in the BA is lower than in EA. Anyhow, butyl acetate may get sold as a general-purpose cleaning solvent but as I say, I know nothing of the Australian retail market and understand you may have something of a nanny state problem at least as bad as the EU!
That sound great! I'll start reading the nail polish labels to find one without Acetone!For the ethyl acetate you may need to distill your own from nail polish remover. Check the ingredients to make sure if it has ethyl acetate and NOT acetone. You can then make a 'DIY' distillation setup and get fairly pure solvent. You will need to salt brine wash to help separate the water and solvent. And distill the solvent to remove the minor impurities. Here in Brasil the nail polish removers you can recover around 40-45% ethyl acetate depending on the brand.
sodium carbonate instead of the Ethyl Acetate?You can use sodium carbonate (backed baking soda) with cielo but may end up with goo due to needed a specific amount of water content.
Instead of calcium hydroxide, as the base.sodium carbonate instead of the Ethyl Acetate
Fabulous - I totally forgot about the nail polish remover, despite having several bottles lined up for exactly what @modern says!That sound great! I'll start reading the nail polish labels to find one without Acetone!
sodium carbonate instead of the Ethyl Acetate?
Do you have a solvent you have access to? I personally like xylene over ethyl acetate but I can't find in stores. Maybe limonene would be easier for you to find?Thank you all.
If I won't find any of those, I'll might just try A/B extraction. Sodium hydroxide is easy to find
Would the salt brine fix this? The alcohol dissolves the salt so shouldn't remain in solution with EtOAc are atleast not in double digit percentage. When I went this route I had to wash 3x with saturated salt brine water to pull the impurities and alcohol. Pretty sure all the nail polish with ethyl acetate use alcohol mixed. Distilling removes any additives like oils and fragrance and color. To separate the alcohol is with salt brine.Fabulous - I totally forgot about the nail polish remover, despite having several bottles lined up for exactly what @modern says!
Just bear in mind, if it's commixed with ethanol it can be exceedingly difficult to separate EA from EtOH as they have very similar boiling points.
A/B is quite tricky, easier would be to extract alkaline cactus paste with another solvent (toluene, xylene) and salt out the alkaloid with acidic water.Thank you all.
If I won't find any of those, I'll might just try A/B extraction. Sodium hydroxide is easy to find