spectral_metamorphosis
Rising Star
So first timer here, I followed Cybs hybrid atb salt tek all at room temp but now I'm having trouble getting bigger yields. Im getting maybe a few mg at a time, is there anything else I can do to get some decent yields going? Anything is much appreciated

60 mL is also a fair amount - unless you're using particularly alkaline tap or well water - and certainly enough to ensure whatever amount of DMT is present will remain protonated until the lye gets added. That amount of vinegar corresponds to roughly 3.15 g of acetic acid (if it's the usual 5% acid) which requires about 2.1 g NaOH for neutralisation, so you've definitely added enough lye.