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first time fasa.

Migrated topic.

jaketurn

Rising Star
Hello, I dissolved 1.5g of freebase into 75ml acetone and 450g of fumaric acid into acetone. I mixed the two and right away it turned cloudy white and now I have it sitting at room temp. As this is the first time I have done fasa I was just curious on the way it looks. I read its supposed to be more like little crystals but It looks very small powdery/grainy to me. Like very fine sand. I checked the ph and its about 6. I just wanted to make sure its fumarate and not something else undesirable.
Thanks

EDIT: The acetone evaped and now its just a left over yellow syrup, no crystals. I assume its yellow from left over naptha.
Nevermind I think I solved the problem
 
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