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freeze precip results so far

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OnceKnownNowFlown

Rising Star
Merits
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Hiya guys.

So I left it to precip till morning, about 8 hours and this is what I've got so far. Curious about the big white glob, guess it can all be dried and cut up?
I realised there was waaaay too much solv for the tray so have poured some into another container to keep the level low.

Can I evap after freeze precip? It's hot here at the moment and could take advantage of the weather :)

Pics to be added asap.
 

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Hey OKNF

The blob could be a water drop that has frozen...you will see if it melts later.
You really need 18-24hrs to be sure all the spice has precipt'd out...
I would just re-use the Nap for another pull or store for later...It shouldn't hold any more spice and would be a waste to evap to air..:d

If you mean can you evap the crystals after the nap is poured off...then I would recommend using a fan to quickly dry them....they will dissolve back into any remaining nap at warm temps..quicker the better..
 
Hopefully you can see the picture? Just making sure everythings looks alright so far.

Hey Cyb! Anything I can do about the globule? I am gonna be leaving it all in the freezer till about nine or ten tonight (24 hours then) and see what's what. I did manage to have a look at the naptha side on, looked very saturated/milky, so hoping for the best :)
 
OnceKnownNowFlown said:
Hey Cyb! Anything I can do about the globule? I am gonna be leaving it all in the freezer till about nine or ten tonight (24 hours then) and see what's what. I did manage to have a look at the naptha side on, looked very saturated/milky, so hoping for the best :)

Just leave it all as it is...see whats what later..if it is ice its no problem.
 
50g MHRB and about 45ml in each pull, total of 3 pulls - I will take another picture now :)

Edit: I realised there was too thick amount of solvent (or so I thought) and decided to move some to another container, so hopefully I will yeild more that what is just in the baking try above, later on/tomorrow :)


Seems to be a slightly sticky looking residue in there too. Guess its still the naptha?!
 

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cyb said:
OnceKnownNowFlown said:
Seems to be a slightly sticky looking residue in there too. Guess its still the naptha?!

You will get some sticky in there as well..cant be helped though...just dry,dry,dry with a fan. It will all mix up when you scrape.
Nice white xtals though :d

hey, yeah they came out great. my scales aren't brilliant, but it weighs 200mg... thats not even a starter on what i have in the freezer at the moment, expect about a gram or just over :) hopefully i will feel okay tomorrow to take the step up... (that white glob was ice!)
 
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