Help please

[Sooodacandan]

Extracted 100g of mhrb. Used 100g lye, 250ml distilled water, 50ml of warm naptha on 3 slow jar rolls (no emulsions) per jar Waited 10-15 min between rolls. Did this 3 different times. Freeze precipitation over night, at least 18 hrs in freezer. Nothing came back.
I didn’t have the video usually watched so the amounts were done by memory. ThisHas been done before with a yield of at least .8-.9
Did something get mis judged on amounts of X or did bark go bad? It’s only a month old shredded.
Lastly, can it be saved by repulsing again? or is it lost? Because just don’t know what to do and at a loss as to where to go from here. Thanks

 

[bezevo]

Have you used this same batch of bark before or is it a new batch ?

and have you saved everything /soup ...in case the goods still there ?
Never throw away anytthing in case it was an error and you can recover later .

Good bark sould be good for decades .

Sometimes if the naptha is no sachairated enough you could evap 40% and try freeze precept again .

and is your freezer below -0f


good luck

 

[Sooodacandan]

It’s the same batch of bark I’ve used before . It’s only 3 weeks to a month old. Yes I still have soup and I still have naptha I extracted in the freezer

 

[Sooodacandan]

Yes freezer is

 

[Sooodacandan]

The funny thing is it was cloudy when I was doing third pull (having it in the freezer between pulls)

 

[Sooodacandan]

The only thing I can think of is my water bath not being hot enough or my surroundings weren’t warm enough. I was hanging out in a shop and it was kinda cool. I was using a hot plate to keep water warm

 

[TransistorBass]

Sachairated = Saturated

I literally had to type it because in my head i wasn't sure how to spell it @bezevo

Once in a while I have a brain fart and spell 'Special' as Speshial, then I have a word with myself!

 

[Sooodacandan]

I had the same thing happen to me yesterday lol

 

[Sooodacandan]

So am I on the right path for my issue:
1, evaporate with air what I got on the naptha and see what I got
And/or
2 do the above and add say 60g or so lye to soup and try again under warmer naptha conditions.
This has had to have happened to someone else and came up with a solution. Maybe?

 

[fractals4life]

I see no need to add 60g lye to 250ml water that already has 100g in it! That;s way too much already.

Sounds like not enough jar rolling, you need the soup and naphtha to mingle intimately in order for the DMT to dissolve in the naphtha.
I usually invert the vessell ( which is 3/4 full ) and back again, with a cadence of one inversion every 3 seconds or so, a few times and then wait for it to separate fully before doing that again five times. Look out for emulsions starting to form when waiting for it to separate and back off on the vigour of mixing if you see that.

Also 250ml water sounds V low for 100g bark, I usuallly have a volume of about 750ml of soup for 50 or 100g of bark runs.

Good luck!

 

[Sooodacandan]

Thank you for the help. I am going not add any more lye and do another extract with fresh nap. I’ll lyk how she goes. Thank you again wholeheartedly