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nafta status after 6 months... ideas? : )

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DarylDee

Rising Star
Merits
42
Hi Brothers!!

How're you in your dimensional space?
It's so nice to come back here, I was not a big writer, but after a while moving in curious places with curious reasons I'm back to my home town for a while to meditate abt and metabolize the events that changed and changing me.

Btw, to cut the long story short (I know somebody loves long stories ;p ), I would love to show you a pic and discuss together.

Well, this was what happened 6 months ago.
During a STB extraction tek I've obtained after the first tentative a naphtha not really pure that lead crystals to back melting after took out from the freezer.
Unluckily this "freezing-defreezing" process didn't left any chance to the freebase to stay solid except for few micro grams.
I tried many ways to frost and defrost, saturation and ammonia washes, sodium carb washes, re-x and nothing.
The main problem was the first naphtha type.

Then I tried other solvents and following strictly the FAQs i got into a sufficient result.
My country have a BIIIIG lack of substances provisioning.

Now I'm back with all the necessary, included some my new toys (one pict is there, i love this separatory funnel so muuuuuuch).

What I want to show you and discuss is one jar of naphta I saved knowing that contains a loooot of DMT.
I cooked approximatively 250g of MHRB and after many pulls (in different STB teks) that's the result.

Now, I remember approx. that this final compound passed through:
naphtha mixes:
octane / hexane / white petrol(standard naphtha ) / xilene(?)
Cleaners:
Sodium Carbonate / Sodium bicarbonate (doing it wrong)
Bases:
Baking Soda 99.9%
Acids:
Vinegar.

Ok, that's the mix, but I made some re-x and I got a nicely saturated liquid that precipitates but in an oily result.


My question to you brothers is: what is this???
How do you think I can try to precip this liquid? What do you think is the right naphtha?
Looks OIL and Solvent.

Thanks a loooot to your ideas and opinions!
And, sorry for the mess : )
I'll improve my english writing hopefully : )

Love and Light!!!
 

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