naptha freeze-technical question-?

[vineseeker]

This time I have almost a liter of saturated naptha in the freezer and I ask myself how long until dmt is out. Have it 24h in there but not much came out, after i take the naptha out of the freezer it goes milky again but in the freezer it is clear?
Any idea if I should take it out? Is the milky color still the dmt in there?

Thanks

 

[alert]

Unless you did a huge extraction you don't have 1L of saturated solvent. Evaporate it down a bit and try precipitating again.

 

[vineseeker]

it was a lot of bark, but I did forget the evap before freeze so that might be a solution.

 

[Du57mi73]

Evap half of it and refreeze.

 

[vineseeker]

Evap half of it and refreeze.

done, much more dmt after prezip. I did another half evap to be sure I get all.