xylene or acetone distill

[congo]

If i do stb then xylene,then do a/b on xylene then extract with acetone.Do you think that it would be easyer to distill the jungle from acetone than a vacuum distill of xylene.
And when i am looking into this DISTIIL what am i looking for
the boiling point of acetone/XYLENE and dmt?
or the vap point of dmt and the boiling point of the liquids,when i am distilling this things.or do i look for the boiling point of dmt/jungle.i know jungle doesnt have proper boiling (as far as i know) point but i will have to use dmt physical properties.
thanks

 

[Dorge]

Good question...

 

[Noman]

Don't distill xylene or acetone with heat unless you're in a fully equipped chem lab.
How are you going to extract from an A/B with acetone? It's miscible with water.

 

[dg]

distilling volatile liquids is easy, but super dangerous for inexperienced chemists to do at home as Noman said. if you are well equiped. then there is lots of easy info to find using g00gle about boiling points
anyways, why not just salt out the np with acid and water wash, then convert back to base if thats what you want.

 

[congo]

i was going to use a hotplate.and perhaps do it outside infact deffantly outside with xylene.and wear serious protection.i thought a crash helmet for the head.
Norman
How are you going to extract from an A/B with acetone?
o i had forgot that point.so i have made a balls up sorry.

dg
why not just salt out the NP with acid and water wash, then convert back to base if thats what you want.
please can you explain from this point.i have my jungle .now what?
i read this bit and i think it is a a/b isnt it.?what you sugested DG
so i have jungle in base form.i dont really want to use xylene because i dont want to just evap that(allthough i am now thinking what the hell i might just evap it) AND I CAn not use actone at this point because its miscible with water.i dont know i might just evap xylene.
and i do KNOW the FASA rounte but i wonder about the losses using FASA on jungle and weather it is still exactly jungle after FASA.
THANKS

ALSO even though acetone is miscible with water what happens if i go ahead wITH the lye/jungle mix and throw some acetone on this.Will the jungle still come over into the acetone.So i have jungle/water/actone.and if this is possible could i easy get jungle out from the this mix.