• Members of the previous forum can retrieve their temporary password here, (login and check your PM).

DIY Soxhlet body

Migrated topic.

k.neo

Rising Star
This time got myself into making a Soxhlet body, I have acquired a cheap 50cm long, glass Graham condenser to put on top of the body. All copper piping, body 2", leg 1" pipe, vapor 1/2", 1/4" gas thin walled tube for solvent cycle. The cycle level is adjustable by means of lengthening or shortening the the return pipe using a flexible transparent tube of various length (not pictured). If I use a long piece of tubing to join the 2 smaller tubes the cycle would be longer, you get the idea. A clear tube allows watching the level of solvent in the system.
Top cap is to be secured with some Teflon tape.

Soldering was made is this order, 2" cap on the body, the leg, top vapor nipple then lower (then drilled out holes and cleaned), completed vapor tube, drilled out a hole in the corner of the 2" cap to secure the solvent tube lastly the solvent return.

The soldering paste was cleaned with tissue papers while the pieces were still hot after soldering. Some cleaning probably needed to remove traces of paste.
 

Attachments

  • 20190313_152858.jpg
    20190313_152858.jpg
    417.9 KB · Views: 0
  • 20190313_152845.jpg
    20190313_152845.jpg
    451.5 KB · Views: 0
  • 20190313_153416.jpg
    20190313_153416.jpg
    468.5 KB · Views: 0
  • 20190313_154626.jpg
    20190313_154626.jpg
    289.5 KB · Views: 0
  • 20190313_161957.jpg
    20190313_161957.jpg
    359 KB · Views: 0
  • 20190313_165313.jpg
    20190313_165313.jpg
    665.6 KB · Views: 0
  • 20190313_165340.jpg
    20190313_165340.jpg
    229.7 KB · Views: 0
  • 20190313_165508.jpg
    20190313_165508.jpg
    330.9 KB · Views: 0
  • 20190313_174334.jpg
    20190313_174334.jpg
    509 KB · Views: 0
  • 20190313_174344.jpg
    20190313_174344.jpg
    257 KB · Views: 0
Back
Top Bottom