TEK Ethyl acetate approach [CIELO]

[Ruffles]

I was going over the wiki and there is little information on solubility of different forms of mesc in solvents, in fact it claims dmt fumarate is soluble in water. That needs some updating.

On our hands, the solubilities of mesc malate and fumarate in water are ridiculously low. We could only get 100 mg of mesc fumarate dissolved in 2 mL of 80 Celsius water with lots dropping out of solution as it cooled to room temp, solubility then at <50 mg/mL. Mesc malate is slightly more soluble, at room temp <70 mg/mL. This was unexpected.

Anyone has an estimate of mesc citrate solubility in water?

 

[nikolas]

Try adding fresh EA (start with 100ml), it should dehydrate your gooey layer and xtalize eventually. You may need to add up to 250ml.

I Add 100ml now i wait if you know wich is my bridgessi i will post pisture.
Thanks for replaying

 

[Quetzal7]

Hey
I just tested with fumaric acid, and to decided to do a side to side with mono citrate
I just divided the solvent in half after pulling

Results :
1.47% mono citrate
0.85% fumarate = 1.26% fumarate

On 200g batch.
I find this is rather significant difference, and i did it quite carefully
The efficiency of fumarate has been tested empirically before?