piperine tek help!!!

[remediosvaro]

i did the piperine rubbing alcohol then precipitation tek exactly as it said too. as soon as i added the water the solution turned milky and went from transparent to white. then i poured the solution through a filter, but nothing got caught?! the solution on the other side of the filter was just as white as the original and the filter was clean.


what can i do to make these crystals bigger?! i now have about 7x as much liquid as i did in the beginning, and i need to find a way to separate the alks.


please help, its urgent!