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Post SWIM's Yeilds !
- Thread starter El Ka Bong
- Start date
Garden Dave
Esteemed member
Garden Dave
Esteemed member
11.9 grams from 500g of the best darn bark ever.
Garden Dave
Esteemed member
1000g MHRB
STB
1st Pull 500ml Naptha Fan evap 3.5g
2nd Pull 509ml Naotha Fan evapwd 5.4 g
8.9g 2 pulls elapsed time 3hrs
STB
1st Pull 500ml Naptha Fan evap 3.5g
2nd Pull 509ml Naotha Fan evapwd 5.4 g
8.9g 2 pulls elapsed time 3hrs
Garden Dave
Esteemed member
Garden Dave
Esteemed member
Yeah this was just teaching a friend the quick and dirty mudpie method.ngl, freeze precip was far prettier… yield was way better too
Garden Dave
Esteemed member
Heptane vs napthangl, freeze precip was far prettier… yield was way better too
Famili-a-rentity
Esteemed member
0,81 g (0,81%) yield from 100 g MHRB (Brazil), via ATB Max Ion Tek, 6x naphta heated pulls, than freeze precip. 95% white cristals. Some bigger chunks remained after shredding the bark. Next time I will shred with a milkshake blender, after soaking. I hope it helps make it way smaller, rising the result.
After pulls I did one extra pull with xilol. The evaporation is in progress, so more goodies (some red colored jungle spice) I expect. My plan is making a solution with citric acid, so will be consumable via oral route. I wont know how much actives will be in this extra product. I tried once like a pharma and it has a decent effect!
After pulls I did one extra pull with xilol. The evaporation is in progress, so more goodies (some red colored jungle spice) I expect. My plan is making a solution with citric acid, so will be consumable via oral route. I wont know how much actives will be in this extra product. I tried once like a pharma and it has a decent effect!
c.a.c.t.u.s
Established member
How much nps and naoh and h20 were involved in this?
Alev-Kev
Just a consciousness walking around in a meatsak
4.63 from mini a/b. Still some left in the jars to pulls. Starting amount was like 10g. I learned i couldn't do all of that in one jar 
One love
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WalterChronkite
Esteemed member
Just shy of 4.5g from 200g MHRB using some variation of the max ion Tek. Some small portion of that could have been carry over from previous failed attempts at ACRB. Hardest .3g ever pulled let me tell you.
Currently running another batch of 200g of the same MHRB loosely following max ion, except this time I used 0.2 M HCL (vinegar previously) as the acid soak (similar to method 2 in this paper), followed by vacuum filtration through a Buchner filter, and a 3x shake and settle naphtha defat step. Salted tonight and I'll base and pull tomorrow. Curious to see if it'll make any difference in yield, crystal quality or ease of pulling, mostly just fooling around as it keeps me busy. I want to make some ejuice and also some different enhanced leafs, so grams go quick down that road.
Currently running another batch of 200g of the same MHRB loosely following max ion, except this time I used 0.2 M HCL (vinegar previously) as the acid soak (similar to method 2 in this paper), followed by vacuum filtration through a Buchner filter, and a 3x shake and settle naphtha defat step. Salted tonight and I'll base and pull tomorrow. Curious to see if it'll make any difference in yield, crystal quality or ease of pulling, mostly just fooling around as it keeps me busy. I want to make some ejuice and also some different enhanced leafs, so grams go quick down that road.
WalterChronkite
Esteemed member
I was being lazy not wanting to email it to myself. Someone said mason jars were the way to go... I am unconvinced.
The way to go in what regard?
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WalterChronkite
Esteemed member
For crystallization. Trying to scrape those jars was pretty bad. I ended up just getting most of it and just hit it with a little more NPS to redissolve it. I've tried the glass food containers with plastic lids with silicone seals, they seem fine, but the plastic is probably warping.
Just slow evap in a tapered shot glass to make one huge xtal jk lol.
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One love
WalterChronkite
Esteemed member
So I finished evaporating my first three pulls from the above and beyond method above (filter, defat, 0.2 M HCL). Just under 2 grams. But boy is it clean and powdery. All in all seems like it will be less of a yield weight wise. Not sure how much of the difference is going to be DMT vs other stuff. Haven't tried the new batch to compare, probably too subjective to draw any conclusions. But if you want nice clean crystals, and have a Buchner filter, give it a roll.
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