What if...

[Z E D]

... SWIM takes the fourth pull soon (15min.) after shaking...

He saw that the last NP solvent pull should stay for about 4 days to get the last crystals, but everytime he let the NP solvent (he uses petroleum ether) more time than unusual, in any batch, he see more yellow stuff so...

If he takes 4th batch as the other, will he has the same results?

 

[acolon_5]

... SWIM takes the fourth pull soon (15min.) after shaking...

He saw that the last NP solvent pull should stay for about 4 days to get the last crystals, but everytime he let the NP solvent (he uses petroleum ether) more time than unusual, in any batch, he see more yellow stuff so...

If he takes 4th batch as the other, will he has the same results?

That's the trade off. The longer the NPS sits in the mimosa wine, the more fats end up in the final product. That's why I do an A/B with a defat. I can leave my NPS in the jug for weeks on end without getting much, if any, discoloration. If you pull after only 15 minutes, you won't get very much out.

I suggest freeze precipitating the first 3 pulls together and doing a seperate freeze precipitaiton on the 4th pull (BTW I do like 5-6 pulls and STILL get spice coming out). That way you have 2 batches, one cleaner than the other.