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extraction

  1. dolven

    DMT crystalization in acid-base extraction

    SWIM has been reading many different teks, and working hard to learn about the chemicals he could potentially use, and already seems to have a mescaline extraction well figured out, heavily based off of the KASH's A/B mescaline extraction tek. He has learned a lot about it the past few days, and...
  2. T

    Found 2+ yr old bark + lye soup

    Hello, I'm new here. Just wanted to get some thoughts on an old mix I have. I'm not sure exactly how long it's been under my sink forgotten, years for sure. Back then had some mhrb bark lye mixture and realized I had very little naptha. So I decided to pour the soup into the naprha can and...
  3. A

    Which Ultrasonic Homogenizer Tek for pulling?

    Good Day My Friends. I woke up a few days ago and decided that I want to learn how to do a DMT pull with the ultrasonic equipments that I currently have. I have experience with Cannabis extraction via super critical CO2, Ethanol, Short Path Distillation and other various methods. I have been...
  4. the_Architect

    Why is it so red spice? nice shield

    QUESTION: Why so reddish/brown? Is it good for consumption? Would you re-crystalize it? how? I tried my usual extraction path, cyb´s A/B max ion tek. Mimosa hostilis rootbark and Heptane as solvent But this time, I tried filtering the MHRB material with a cheese cloth (actually and old...
  5. thevista

    Extraction questions

    Hello. I’m new to DMT. I have searched for the TEKs and because of the geographical issues I only have access to specific materials to extract DMT. Which are; 1- Hexane 2- Naoh (Sodium Hydroxide) 3- MHRB <MOD EDIT - No Sourcing Talk!> I’ve never done extraction before and I’m afraid I could...
  6. F

    Adding more water to Soup

    Hello every space traveler out there. I have a question. So, I already added Naptha to the Soup and did all required steps like heating the soup in a warm bath with the Naptha mixed with the lye and mimosa powder. Here's the thing ; The Naptha that I see is around 20 ML and I added 80 ML of...
  7. G

    TEK Looking for advice/comments on extraction

    Hi Using lazyman's/nomans teks since around 2010, I now tried with 100% xylene for the first time. Evap test completely clean, but it takes a long time to evaporate. I started with 50g powdered (very, very finely powdered!) MHRB, 75g NaOH, 0,5l water and used 20 to 30ml room temperature...
  8. Subtlevibrations

    How long is bark solution “okay”? (Jungle Spice)

    I have some basified mimosa soup left over from a STB extraction I finished about 4 months ago. I’ve been sitting on the left over soup, as I intend to pull from it using toluene to extract some jungle spice. How long can I let the bark soup sit and still safely pull from it? Is there any time...
  9. Perlon

    Extracting DMT from Mimosa Hostilis properly

    Hello everyone, I would like to extract DMT from Mimosa Hostilis and am not satisfied with my first attempt. The end product is more of a powder than crystals and the effect is also somewhat disappointing. My throat hurts a lot after smoking and I have no auditory hallucinations and just few...
  10. C

    Residual Naptha Evaporation

    I just did my first DMT extraction and I'm now trying to get the residual Naptha to evaporate from the crystal left in my Pyrex dish. It seems a little oily and I'm wondering if there are any tips or tricks to getting it to evaporate. I've dumped the bulk of the naotha back into my plant matter...
  11. T

    DMT ethanol extraction from DMT & calcium hydroxide slurry.

    Someone suggested that basifying a crude xylene extraction with Ca(OH)2 and drying it would allow one to extract the DMT freebase from the slurry, leaving behind the Ca(OH)2 and calcium acetate (having used acetic acid for the aquesous phase) as they are not soluble in ethanol. Now, what's...
  12. T

    N-oxide solubility in water and DMT from DMT-N-oxide separation with H2O

    On thttps://wiki.dmt-nexus.me/Psychedelic_Compounds_Chemical_and_Physical_Properties#DMT_N-Oxide "...Soluble in water..." without further info is stated. If someone had obtained a "full spectrum" extraction with xylene containing DMT and its N-oxide, could plain distillied water be used for...
  13. Self-container

    Mask(s) for DMT extraction

    I have found two threads on this matter already, though the links provided were dead. As far as content go, they simply mention that one needs a P3 mask, which is a mask that has the highest safety rating. As such, a P3 mask can be many different things. Although a mask with a P3 rating does...
  14. Self-container

    Techniques for evaporation

    I have never extracted DMT before, and whenever I read TEKs, I find myself most hung-up on the evaporation step (if applicable). I wonder how to do it, practically. First of all, I wonder what temperature to have; though that would depend on the non-polar solvent used, so I guess I can just...
  15. S

    Better STB

    So I read the Lazymans Tek and saw that he had gotten 1g out of a Lb of rootbark his first pull which is way to little. Try this. Put 2Kg powdered root bark in bucket, Add three pounds lye and a gallon of water, Stir 3 to 5 min the high amount of lye will cause the water to get extremely hot and...
  16. T

    Is there a limit to reducing (concentrating) acid pulls from MHRB?

    Is there any limit to how concentrated one could get the acid pulls from MHRB? I suppose the lower the volume, the easiest it should be to actually pull the compounds of interest with non-polar solvent after basifying, but is there a maximum level of thickness/viscosity I should stay clear of?
  17. Re-x-ed with acetone

    Re-x-ed with acetone

    The most neon yellow DMT I ever extracted. Probably lots of Oligomer going on since I heated the solution to 65C on my hotplate stirring bar. With the knowledge from the thread from Loveall I will not do that again. 26C max heating with silvent solvent on top (that has a boiling point of only 32C.
  18. pete666

    STB Mescaline Extraction TEK

    Main purpose of this TEK is to have emulsion-free procedure which leads from cactus matter to pure white mescaline when followed properly. This TEK is based on this topic describing emulsion-free procedure for initial extraction and adds salting/titration and further purification. So now it can...
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